Using three different approaches of OSL for the study of young fluvial sediments at the coastal plain of the Usumacinta–Grijalva River Basin, southern Mexico

We use three different approaches of optically stimulated luminescence (OSL) to study young fluvial sediments located at the main channels of one of the largest fluvial systems of North America: the Usumacinta–Grijalva. We use the pulsed photo-stimulated luminescence (PPSL) system also known as portable OSL reader, full OSL dating and profiling OSL dating in samples extracted from vertical sediment profiles (n = 9) of riverbanks to detect changes in depositional rates of sediments and to obtain the age of the deposits. The results of the PPSL system show that the luminescence signals of vertical sediment profiles highly scattered from the top to the bottom contrast with the luminescence pattern observed on well-reset sequences of fluvial deposits where luminescence increase from the top to the bottom of the profile. The profiling and full OSL ages yielded large uncertainty values on their ages. Based on the inconsistencies observed in both ages and luminescence patterns of profiles we suggest that these fluvial deposits were not fully reset during their transport. As an explanation, we propose that in the Usumacinta and Grijalva rivers the cyclonic storms during the wet season promote the entrainment of large volumes of sediments due to high-erosional episodes around the basin resulting from hyper-concentrated and turbid flows. We conclude that the PPSL, profiling and full OSL dating of sediments are useful tools to quantify and to assess the depositional patterns in fluvial settings during the Holocene. These techniques also can yield information about sites where increases in the sediment load of rivers may produce poorly resetting of grains affecting the results of OSL dating

Preserving the palaeoenvironmental record in Drylands: Bioturbation and its significance for luminescence-derived chronologies

Luminescence (OSL) dating has revolutionised the understanding of Late Pleistocene dryland activity. However, one of the key assumptions for this sort of palaeoenvironmental work is that sedimentary sequences have been preserved intact, enabling their use as proxy indicators of past changes. This relies on stabilisation or burial soon after deposition and a mechanism to prevent any subsequent re-mobilisation. As well as a dating technique OSL, especially at the single grain level, can be used to gain an insight into post-depositional processes that may distort or invalidate the palaeoenvironmental record of geological sediment sequences. This paper explores the possible impact of bioturbation (the movement of sediment by flora and fauna) on luminescence derived chronologies from Quaternary sedimentary deposits in Texas and Florida (USA) which have both independent radiocarbon chronologies and archaeological evidence. These sites clearly illustrate the ability of bioturbation to rejuvenate ancient weathered sandy bedrock and/or to alter depositional stratigraphies through the processes of exhumation and sub-surface mixing of sediment. The use of multiple OSL replicate measurements is advocated as a strategy for checking for bioturbated sediment. Where significant OSL heterogeneity is found, caution should be taken with the derived OSL ages and further measurements at the single grain level are recommended. Observations from the linear dunes of the Kalahari show them to have no bedding structure and to have OSL heterogeneity similar to that shown from the bioturbated Texan and Florida sites. The Kalahari linear dunes could have therefore undergone hitherto undetected post-depositional sediment disturbance which would have implications for the established OSL chronology for the region

On the Combination of Logistic Regression and Local Probability Estimates

In this paper we give a survey of the combination of classifiers. We briefly describe basic principles of machine learning and the problem of classifier construction and review several approaches to generate different classifiers as well as established methods to combine different classifiers. Then, we introduce our novel approach to assess the appropriateness of different classifiers based on their characteristics for each test point individuall

Radiocarbon and blue optically stimulated luminescence chronologies of the Oitavos consolidated dune (Western Portugal)

The dune of Oitavos, the underlying paleosol, and Helix sp. gastropod shells found within the paleosol were dated using a combination of radiocarbon and blue optically stimulated luminescence (OSL). The organic component of the paleosol produced a significantly older age (~20,000 cal BP) than the OSL age measurement (~15,000 yr), while 14C age measurements on the inorganic component and the gastropods produced ages of ~35,000 yr and ~34,000 yr, respectively. Rare-earth element analyses provide evidence that the gastropods incorporate geological carbonate, making them an unreliable indicator of the age of the paleosol. We propose that the 14C age of the small organic component of the paleosol is also likely to be unreliable due to incorporation of residual material. The OSL age measurement of the upper paleosol (~15,000 yr) is consistent with the age for the base of the dune (~14,500 yr). The younger OSL age for the top of the dune (~12,000 yr) suggests that it was built up by at least 2 sand pulses or that there was a remobilization of material at the top during its evolution, prior to consolidation

Testing Luminescence Dating Methods for Small Samples from Very Young Fluvial Deposits

The impetus behind this study is to understand the sedimentological dynamics of very young fluvial systems in the Amazon River catchment and relate these to land use change and modern analogue studies of tidal rhythmites in the geologic record. Initial quartz optically stimulated luminescence (OSL) dating feasibility studies have concentrated on spit and bar deposits in the Rio Tapajós. Many of these features have an appearance of freshly deposited pristine sand, and these observations and information from anecdotal evidence and LandSat imagery suggest an apparent decadal stability. The characteristics of OSL from small (~5 cm) sub-samples from ~65 cm by ~2 cm diameter vertical cores are quite remarkable. Signals from medium-sized aliquots (5 mm diameter) exhibit very high specific luminescence sensitivity, have excellent dose recovery and recycling, essentially independent of preheat, and show minimal heat transfer even at the highest preheats. These characteristics enable measurement of very small signals with reasonable precision and, using modified single-aliquot regenerative-dose (SAR) approaches, equivalent doses as low as ~4 mGy can be obtained. Significant recuperation is observed for samples from two of the study sites and, in these instances, either the acceptance threshold was increased or growth curves were forced through the origin; recuperation is considered most likely to be a measurement artefact given the very small size of natural signals. Dose rates calculated from combined inductively coupled plasma mass spectrometry/inductively coupled plasma optical emission spectrometry (ICP-MS/ICP-OES) and high-resolution gamma spectrometry range from ~0.3 to 0.5 mGya−1 , and OSL ages for features so far investigated range from 13 to 34 years to several 100 years. Sampled sands are rich in quartz and yields of 212–250 µm or 250–310 µm grains indicate high-resolution sampling at 1–2 cm intervals is possible. Despite the use of medium-sized aliquots to ensure the recovery of very dim natural OSL signals, these results demonstrate the potential of OSL for studying very young active fluvial processes in these settings

Luminescence Dating of Sediments from Ancient Irrigation Features, and Associated with Occupation of the Hinterland around Anuradhapura, Sri Lanka

This study supports a new investigation into the development and decline of irrigation and associated human activity in the Anuradhapura Hinterland, Sri Lanka (section 2). Optically stimulated luminescence (OSL) age determinations have been made for a variety of sediments from bund and tank systems, irrigation channels, palaeosols and ceramic scatter horizons in the Anuradhapura hinterland (section 3). The geomorphological and archaeological significance of the age determinations has been reviewed in the light of the luminescence results and the samples’ depositional contexts, to constrain the deposition/formation dates of the sampled sediments integrate the OSL results with independent archaeological and historical expectations (section 6). A total of 26 age determinations were made (section 5.3). Dose rate determinations were made using thick source beta counting, high-resolution gamma spectrometry, field gamma spectrometry, measured water contents and calculated cosmic dose rates (sections 4.2.1, 5.1). Equivalent dose determinations were made (sections 4.2.2, 5.2) using the OSL signals from sand sized grains of quartz separated from each sample. Dose rates ranged from 1.1 to 5.0 mGy/a, equivalent dose values ranged from 0.29 to 33 Gy. Age estimates for these samples ranged from 0.14 to 13 ka, the average being 2.9 ka ± 3.1 (section 5.3). Uncertainties on the age estimates were commonly 7% at one standard error. The OSL age estimates from the largest bund and some ceramic scatter sites were greater than 2000 BC. This is older than expected on archaeological grounds and further investigation of these sites may be warranted. The OSL results from the other samples in the present study date bund construction during the initial urbanisation of Anuradhapura c. 400BC, coincident with the major Nachchaduwa bund construction c. 300AD, and in the Late Iron Age / Early Mediaeval period c. 600AD. They date abandonment of one irrigation channel to the 8th Century AD and its infill up to the late 10th Century when Anuradhapura was finally sacked. A further 8 age estimates, from silts and colluvium, relate to the collapse of infrastructure in the Anuradhapura hinterland during the 10th century and continued landscape response during the 11th century, followed by the lead-in to restoration of the irrigation system during the colonial era

Luminescence dating of dune sand and sabkha sediments, Saudi Arabia

32 sediment samples recovered in April 2008 from active and relict dunes, and sabkhas/playas, in Saudi Arabia, were investigated using Optically Stimulated Luminescence (OSL) methods. This work follows an earlier investigation of similar sites over a larger area. The results of the current investigations are reported here. The sabkha and shoreline samples show ages ranging from very modern (with no measurable OSL signal) to 7.6ka, indicating that this study area appears to have some sabkhas significantly younger than those observed in the earlier work. One petrified dune sampled in this work produced an OSL date of 830±210 years, which is consistent with the age ranges of the petrified dunes sampled in the earlier work. Another showed very modern (with no measurable OSL signal) for the indurated sand at the top and an age of 200±150 years for the sand at the back of the dune; another sample taken nearby had an OSL age of 720±180 years. This dune appears to be much younger than the petrified dunes sampled in the previous study. Samples from low-rolling dunes in this study have ages between very modern and 580 years. A barchan dune sample had an age of 60±30 years, similar to ages for barchan dunes sampled in the earlier work. Samples from a low hill had ages of 2.5±0.3 and 5.7±0.5 ka. A buried dune was sampled, producing no measurable natural OSL signal

OSL Characterisation of Two Fluvial Sequences of the River Usmacinta in its Middle Catchment (SE Mexico)

The report summarizes luminescence profiling, initially using a SUERC PPSL system in Mexico, and laboratory analysis at SUERC, used to characterise the stratigraphy and interpret sedimentary processes in terrace deposits of the Usumacinta River, SE Mexico. This was then followed, by quantitative quartz OSL SAR dating of five sediment samples, aimed at defining the chronologicalframework of two sedimentary sequences, USU13-1 and USU13-2. In the wider region, the middle catchment of the Usumacinta River, contains numerous archaeological sites dating to the Maya Classic Period, including Bonampak, Yaxchilan and Piedras Negras. The broader aim of the investigation is to assess whether the two fluvial sequences contain a proxy record of environmental change through the archaeological period of interest. Initial luminescence profiling revealed that the stratigraphy in each profile was complex, reflecting multiple cycles of deposition, with signal maxima, followed by tails to lower intensities, possibly indicating deposition during extreme flood events, interleaved with periods of slower sedimentation, and potentially better luminescence resetting. Laboratory profiling reproduced the apparent maxima/trends in the field profiling dataset, confirming that both sections record complex depositional histories. Furthermore, the variations in stored dose estimates, and luminescence sensitivities with depth, confirm that the sections do not record simple age-depth progressions. Quantitative quartz OSL SAR dating was undertaken on five sediment samples. Given the information obtained from the field- and laboratory-profiles it is not surprising that the equivalent dose distributions for each sample showed considerable scatter, particularly so for the second section, USU13-2. Nevertheless, throughstatistical analysis, individual quartz OSL SAR ages were obtained for each sample. Individual dates fall into the Mayan Post-Classical Period to early modern Period, with statistical combinations pointing to a late 15th century accumulation of USU13-1, and the 18th century accumulation of the sediment within USU13-2. Interestingly, the three samples from section USU13-2, all show some aliquots which tail to higher equivalent doses; furthermore, in each sample, the mean value determined for this component is similar, suggesting that the sediment sampled in USU13-2, may be sourced from a 15th century or older accumulation upstream

OSL investigations at Hardisty, Alberta, Canada

This report is concerned with optically stimulated luminescence (OSL) dating investigations of sediments associated with, and enclosing artefacts of First Nations historic significance in the Battle River Valley area, near Hardisty, east central Alberta. The OSL ages reported here provide chronological control to the archaeological investigations at this site, led by Rob Wondrasek, which have identified thousands of historical artefacts, including projectile points and lithic fragments indicative of occupation. The investigations were commissioned by Enbridge, ahead of the construction of the Edmonton-Hardisty Pipeline, and form one part of a historic resources impact assessment study, to characterise the archaeological site, and evaluate/mitigate the impact of the pipeline related excavations. This report describes the background to the investigation, sampling, and luminescence analysis undertaken to generate sediment chronologies for the Hardisty sediment stratigraphies. Ken Munyikwa visited the archaeological investigations at Hardisty in June 2014 to sample key stratigraphic units within the sediment stratigraphies for OSL dating. Samples were collected from two profiles: from strata encompassing the artefact-bearing horizon, and from strata immediately beneath and overlying this horizon, thus providing terminus post quem (TPQ) and terminus ante quem (TAQ) on the age of this unit. Samples were submitted to the luminescence laboratories at SUERC for dating in August 2014. All samples were subjected to laboratory preparation of sand-sized quartz, and purity checked by scanning electron microscopy. Dose rates for the bulk sediment were evaluated using analyses of the uranium, thorium and potassium concentrations obtained by high resolution gamma spectrometry coupled with beta dose rate measurement using thick source beta counting. Equivalent doses were determined by OSL from 64 aliquots of quartz per sample using the quartz single-aliquot-regenerative (SAR) procedure. The material exhibited good OSL sensitivity and produced acceptable SAR internal quality control performance. Dose distributions from the aliquots were examined using radial plotting methods. All samples revealed some heterogeneity in their equivalent dose distribution, reflecting variable bleaching at deposition and indicating that each sample enclosed mixed-age materials. Age estimates were based on the weighted mean estimate of the stored dose, which weights the stored dose estimate towards the lowest population of equivalent doses, potentially representing the better bleached (at deposition) component. The quartz OSL ages reported herein for the sand sequences at Hardisty-1 and Hardisty-2, have provided the first means to assess the temporal distribution of artefacts within the Hardisty profiles, and furthermore provide TPQ and TAQ for the inferred occupational phases. The sediment chronologies established for each profile are internally coherent, spanning at HD-01 from 7.8 ± 0.7 ka (SUTL2692) to 11.7 ± 0.5 ka (SUTL2694), and at HD-02 from 4.5 ± 0.2 ka (SUTL2695) to 8.7 ± 0.5 ka (SUTL2697; Table 4-1). TPQ for the occupation of the Hardisty site is provided by SUTL2697 at 8.7 ± 0.5 ka. TAQ for the occupation of the Hardisty site is provided by SUTL2695 at 4.5 ± 0.2 ka

Using Optically Stimulated Luminescence to Unravel Sedimentary Processes of the Usumacinta and Grijalva Rivers (SE Mexico)

This report provides an optically stimulated luminescence (OSL) chronology for sediment collected through terrace deposits of the Usumacinta and Grijalva rivers in SE Mexico. The Grijalva and Usumacinta rivers are susceptible to flooding during the hurricane season (between May and November), affecting the population of the state of Tabasco, and leaving many households at a flood risk. The present study was initiated to obtain an understanding of the sediment processes, rates and frequency of flood events in the past. The report summaries the initial luminescence profiling, using a SUERC PPSL system, and laboratory analysis, used to characterise the stratigraphy and interpret sedimentary processes in each profile, together with the quantitative quartz SAR dating used to define chronologies in each. Initial luminescence profiling revealed that the stratigraphy in each was complex, reflecting multiple cycles of deposition, with maxima, followed by a tail to lower intensities, possibly indicating deposition during extreme flood events, followed by a period in which the sediment was mixed and the luminescence signals reset. The laboratory profiling reproduced the apparent maxima/trends in the field profiling dataset. In the Grijalva section, the profiling samples encompass the full range of variations in the IRSL net signal intensities, re-affirming the complex stratigraphy. In the Usumacinta section, the profiling samples were positioned on the trend of a normal age-depth progression, which may indicate that the horizons sampled are well suited for quartz SAR dating. Given the nature of the sediment sampled, it is unsurprising that the equivalent dose distributions obtained for each of the dating samples showed considerable scatter, leading to some ambiguity in estimating a stored dose for age calculations. In each, a number of aliquots returned high equivalent dose values, implying residual luminescence signals (leading to higher apparent ages), and others, low values, implying re-setting of the luminescence signals in the modern environment. It is well recognised that fluvial sediment of this sort can enclose mixed-age populations. It has been argued elsewhere (Fuchs and Lang, 2001; Lepper et al., 2000; Olley et al., 1998; Olley et al., 1999) that the lowest population of dose(s) may best represent the burial dose of the youngest depositional component, and that an arbitrary value of say the lowest 5% be used in age calculations. However, if this method was instigated for the Mexican samples, it would include the low equivalent dose values thought to reflect contamination from the surface, by bioturbation or some other weathering process, leading to artificially young ages. Therefore, each sample was evaluated on an individual basis, where low equivalent doses were considered to represent contamination and rejected, along with high equivalent dose outliers and any aliquots which failed SAR acceptance criteria. The weighted mean and weighted standard deviation of the reduced set were used in age calculations. The dating results reported here provide a first chronology to interpret the changing fluvial dynamics of the Usumacinta and Grijalva rivers, and a means to quantify flood events through the historical period. The chronology established for the Grijalva section spans from the 6th century AD to the 12th century AD; and the chronology for the Usumacinta section from the 17th century AD to the 19th century AD