Thermal microstructure measurement system

A thermal microstructure measurement system (TMMS) operates autonomously h its own internal power supply and telemeters data to a platform. A thermal array is mounted on a cross-braced frame designed to orient itself normal to existing currents with fixed sensor positioning bars protruding from the cross bars. A plurality of matched thermistors, conductivity probes and inclinometers are mounted on the frame. A compass and pressure transducer are contained in an electronics package suspended below the array. The array is deployed on a taut mooring below a subsurface float. Data are digitized, transmitted via cable to a surface buoy and then telemetered to the platform where the data is processed via a computer, recorded and/or displayed. The platform computer also sends commands to the array via telemetry

Understanding Snow Microstructure for Microwave Remote Sensing

Scientists from the snow and soil remote sensing communities met to build on recent developments in objective snow microstructure measurement techniques by improving the understanding of their application in remote sensing at microwave frequencies

Microstructure measurement and microgeometric packing characterization of rigid polyurethane foam defects

Streak and blister cell defects pose extensive surface problems for rigid polyurethane foams. In this study, these morphological anomalies were visually inspected using 2D optical techniques, and the cell microstructural coefficients including degree of anisotropy, cell circumdiameter, and the volumetric isoperimetric quotient were calculated from the observations. A geometric regular polyhedron approximation method was developed based on relative density equations, in order to characterize the packing structures of both normal and anomalous cells. The reversely calculated cell volume constant, Cc, from polyhedron geometric voxels was compared with the empirical polyhedron cell volume value, Ch. The geometric relationship between actual cells and approximated polyhedrons was characterized by the defined volumetric isoperimetric quotient. Binary packing structures were derived from deviation comparisons between the two cell volume constants, and the assumed partial relative density ratios of the two individual packing polyhedrons. The modelling results show that normal cells have a similar packing to the Weaire-Phelan model, while anomalous cells have a dodecahedron/icosidodecahedron binary packing

Orientation imaging of macro-sized polysilicon grains on wafers using spatially resolved acoustic spectroscopy

Due to its economical production process polysilicon, or multicrystalline silicon, is widely used to produce solar cell wafers. However, the conversion efficiencies are often lower than equivalent monocrystalline or thin film cells, with the structure and orientation of the silicon grains strongly linked to the efficiency. We present a non-destructive laser ultrasonic inspection technique, capable of characterising large (52 x 76 mm2) photocell's microstructure – measurement times, sample surface preparation and system upgrades for silicon scanning are discussed. This system, known as spatially resolved acoustic spectroscopy (SRAS) could be used to optimise the polysilicon wafer production process and potentially improve efficiency

Preparation and Characterization of Barium and Strontium Hexaferrite Employing Recycled Millscale

In this project work, permanent magnet barium/ strontium hexaferrite materials was prepared from millscale, using hematite derived from millscale by the Curie Temperature Separation Technique (CTST). The excellent CTST isolation and purification of wustite,FeO contained in the millscale and converted to hematite,Fe2O3, was confirmed by X-Ray Diffraction (XRD) pattern analysis and element analysis by Electron Dispersive X-Ray (EDAX). The sample was prepared by recycling the waste product from Malaysian steel-making factories. Using a Curie temperature separation technique, the wustite,FeO contained in the millscale was separated by this new technique using deionized water at 90oC/100oC in the presence of 1T external magnetic field. The wustite iv was then oxidized in air at 400oC/500oC/600oC for 10 hours. An XRD phase analysis showed that a very high percentage of Fe2O3 was present in the final powder preparation. A conventional ceramic powder processing method was then carried out to prepare hexagonal BaFe12O19 and SrFe12O19 pallet shaped samples. Analysis of samples was done on density, resistivity, X-Ray Diffraction (XRD), Particle Size Analysis (PSD), Electron Dispersive X-Ray (EDAX), Scanning Electron Micrsocopy (SEM), grain size, saturation magnetization, coercive force and remanence. The effect of prolonged milling time shows a positive tendency for the formation of needle shape microstructure (0.3μm-1μm) of barium hexaferrite. The magnetic properties were measured using an Approximation Method (APM) theory. The 3.33 kG high remanence , 0.74 kG saturation magnetisation and 2.857 kOe coercive force of the sample derived from millscale shows that recycling a waste steel-making product has a high potential to produce a low cost ferrite in the future

Tracer Survey in the Cape Verde Region Traceraufnahme in der Kapverdenregion Cruise No. 10, Leg 1 October 31 – December 06, 2008 Ponta Delgada (Portugal) – Mindelo (Cape Verde Islands)

The research cruise MSM10/1 was extremely successful. All programs were able to collect high quality data and the anticipated goals of the expedition were fully met. We have been able to carry out the first comprehensive survey of a tracer release in the Guinea Upwelling region (GUTRE) roughly seven month after the tracer was released at 8°N 23°W in April 2008. We have estimated that a total of 40% of the tracer was found during this cruise. While the horizontal spreading and mixing was larger than anticipated, the vertical extent of the tracer found was small. The low vertical tracer spreading rate estimates are supported by the micro structure profile data. The extensive survey of the upper 1000m of the oxygen minimum zone (OMZ) allowed comparing our sections with several previous surveys. We found that the lowest oxygen values in the core of the OMZ have dropped at record low values below 40 μmol/kg. The preliminary findings from the trace metal work focused on Fe ligand measurements shows a slight higher excess ligand concentration in the surface (50m) for three stations. The two other stations show a slight decrease at this depth. A large number of biochemical samples were taken and were analyzed in Kiel for DNA and RNA diversity. The tracer release experiment provided an ideal environment for repeated biochemical sampling in the same water mass

Integration of a RSI microstructure sensing package into a Seaglider

Seagliders are a type of propeller-less AUV that glide through the water by changing their buoyancy. They have become mainstream collectors of standard oceanographic data (conductivity, temperature, pressure, dissolved oxygen, fluorescence and backscatter) and are increasingly used as trucks to carry a wide variety of hydrographic and bio-geochemical sensors. The extended sensor capability enhances the utility of the gliders for oceanographic observations. Seagliders are designed and optimized for long-term missions (up to 10 months) and deep sea profiling (up to 1000 m). They provide high resolution oceanographic data with very good temporal and spatial density, in near real-time, at a fraction of the cost of ship collected data. These performance parameters are sometimes at odds with the physical dimensions and electrical requirements of the hydrographic and bio-geochemical sensors scientists want installed in gliders. However, as the acceptance of gliders as an integral component of the oceanographic suite of measurement tools grows so do the efforts of sensor vendors to develop products that meet the size, weight and power requirements for successful glider integration. Turbulence microstructure sensors are one measurement system that scientists desired on Seagliders but that until recently did not fit the glider footprint. In collaboration with Rockland Scientific, Inc., a suite of RSI turbulence microstructure sensors was recently integrated into a Seaglider and the system’s performance validated during field tests in Puget Sound near Seattle, WA and in Loch Linnhe on the west coast of Scotland. Ocean turbulence controls the mixing of water masses, biogeochemical fluxes within them, and facilitates ocean-atmosphere gas exchange. As a result, turbulence impacts global ocean circulation, polar ice melt rates, drawdown of atmospheric carbon dioxide and carbon deposition, coastal and deep ocean ecology, commercial fisheries, and the dispersion of pollutants. Turbulent mixing is also recognized as a key parameter in global climate models, used for understanding and predicting future climate change. Seagliders equipped with turbulence microstructure sensors will allow scientists to map the geographical distribution and temporal variability of mixing in the ocean on scales not possible with ship-based measurements. This presentation discusses the technical aspects of the integration of the turbulence sensor suite on a Seaglider with an emphasis on achieving high data quality, while retaining the performance characteristics of the Seaglider. We will also describe applications for this sensor suite, examine the turbulence measurement data already collected by the Seaglider and discuss future deployment plans

Physical and Biogeochemical Studies in the Subtropical and Tropical Atlantic

Maria S. Merian Cruise Report MSM18/L2 Cruise No. 18, Leg 2 May 11 – June 19, 2011 Mindelo (Cape Verde Islands) – Mindelo (Cape Verde Islands