Cold gas dynamic spraying of metal matrix composite coatings with subsequent friction stir processing

The present study forms an initial investigation in to the development of an innovative process to apply wear resistant surface layers to a chosen substrate material. Tungsten carbide – cobalt chromium, chromium carbide – nickel chromium and aluminium oxide coatings were cold spray deposited on to AA5083 grade aluminium and subsequently friction stir processed. In order to improve the deposition efficiency of the cold spray process, coatings were co-deposited with powdered AA5083. Friction stir processing (FSP) has been used in combination with the cold spray deposited coating to produce an engineered surface layer containing evenly dispersed reinforcing particles that reflects the constituent phases of the feedstock powder. Microstructural characterisation was performed on the test specimens making use of micro-hardness testing, light optical and scanning electron microscopy with electron dispersive spectroscopy to establish the elemental composition of the processed layer. The resulting data was contrasted with as-deposited coatings (no FSP) to highlight the variation in microstructure between the two conditions. The results demonstrate that FSP has improved the dispersal of reinforcing particles within the metal matrix composite layer with the average interparticle spacing decreasing by up to 68%. The micro-hardness of friction stir processed material shows an increase of approximately 540% over the unaltered substrate and 118% increase over the as-deposited MMC layer, in the case of the tungsten carbide reinforced coating

The erosion performance of cold spray deposited metal matrix composite coatings with subsequent friction stir processing

This study forms an initial investigation into the development of SprayStir, an innovative processing technique for generating erosion resistant surface layers on a chosen substrate material. Tungsten carbide – cobalt chromium, chromium carbide – nickel chromium and aluminium oxide coatings were successfully cold spray deposited on AA5083 grade aluminium. In order to improve the deposition efficiency of the cold spray process, coatings were co-deposited with powdered AA5083 using a twin powder feed system that resulted in thick (>300 µm) composite coatings. The deposited coatings were subsequently friction stir processed to embed the particles in the substrate in order to generate a metal matrix composite (MMC) surface layer. The primary aim of this investigation was to examine the erosion performance of the SprayStirred surfaces and demonstrate the benefits of this novel process as a surface engineering technique. Volumetric analysis of the SprayStirred surfaces highlighted a drop of approx. 40% in the level of material loss when compared with the cold spray deposited coating prior to friction stir processing. Micro-hardness testing revealed that in the case of WC-CoCr reinforced coating, the hardness of the SprayStirred material exhibits an increase of approx. 540% over the unaltered substrate and 120% over the as-deposited composite coating. Microstructural examination demonstrated that the increase in the hardness of the MMC aligns with the improved dispersion of reinforcing particles throughout the aluminium matrix

Microstructural evolution in solution heat treatment of gas- atomised Al alloy (7075) powder for cold spray

Cold gas dynamic spray is being explored as a repair technique for high-value metallic components, given its potential to produce pore and oxide-free deposits of between several micrometers and several millimeters thick with good levels of adhesion and mechanical strength. However, feedstock powders for cold spray experience rapid solidification if manufactured by gas atomization and hence can exhibit non-equilibrium microstructures and localized segregation of alloying elements. Here, we used sealed quartz tube solution heat treatment of a precipitation hardenable 7075 aluminum alloy feedstock to yield a consistent and homogeneous powder phase composition and microstructure prior to cold spraying, aiming for a more controllable heat treatment response of the cold spray deposits. It was shown that the dendritic microstructure and solute segregation in the gas-atomized powders were altered, such that the heat-treated powder exhibits a homogeneous distribution of solute atoms. Micro-indentation testing revealed that the heat-treated powder exhibited a mean hardness decrease of nearly 25% compared to the as received powder. Deformation of the powder particles was enhanced by heat treatment, resulting in an improved coating with higher thickness (* 300 lm compared to * 40 um for untreated feedstock). Improved particle–substrate bonding was evidenced by formation of jets at the particle boundaries

Fabrication and microstrain evolution of Al-TiB2 composite coating by cold spray deposition

This paper investigates the microstructure evolution of Al-TiB2 coatings prepared by cold spraying. In situ Al-TiB2 composite powders containing uniformly distributed titanium diboride (TiB2) particles with a size range of 5 to 100 nm in the Al matrix and Al/Al-TiB2 blended powders were used as the cold spray feedstock for coating fabrication on aluminium alloy substrates. The microstructures of the feedstock powders and as-deposited coatings were characterised using scanning electron microscopy with energy dispersive X-ray (EDX) analysis and X-ray diffraction (XRD). Al/Al-TiB2 blended powder coatings, compromising closely packed powder particles, were sprayed to an approximate thickness of 500 μm. Al-TiB2 composite coatings (approximately 50 μm thick) were obtained retaining the microstructure of the composite powders being sprayed and no evidence of detrimental phase transformation was found. However, micro-cracks were found to exist in the Al-TiB2 coating due to the hardly deformable powder particles. Little or no microstrain was revealed in the as-sprayed Al-TiB2 coating, indicating that annealing may have occurred due to the localised adiabatic heating during the spraying process. It is demonstrated that it is possible to fabricate the Al-TiB2 composite coating by cold spray deposition but further improvements to eliminate coating cracking are required

Towards Fully Additively-Manufactured Permanent Magnet Synchronous Machines: Opportunities and Challenges

With the growing interest in electrification and as hybrid and pure electric powertrains are adopted in more applications, electrical machine design is facing challenges in terms of meeting very demanding performance metrics for example high specific power, harsh environments, etc. This provides clear motivation to explore the impact of advanced materials and manufacturing on the performance of electrical machines. This paper provides an overview of additive manufacturing (AM) approaches that can be used for constructing permanent magnet (PM) machines, with a specific focus on additively-manufactured iron core, winding, insulation, PM as well as cooling systems. Since there has only been a few attempts so far to explore AM in electrical machines (especially when it comes to fully additively-manufactured machines), the benefits and challenges of AM have not been comprehensively understood. In this regard, this paper offers a detailed comparison of multiple multi-material AM methods, showing not only the possibility of fully additively-manufactured PM machines but also the potential significant improvements in their mechanical, electromagnetic and thermal properties. The paper will provide a comprehensive discussion of opportunities and challenges of AM in the context of electrical machines

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Microstructural Characterization of Shrouded Plasma-Sprayed Titanium Coatings

Titanium and its alloys are often used for corrosion protection because they are able to offer high chemical resistance against various corrosive media. In this paper, shrouded plasma spray technology was applied to produce titanium coatings. A solid shroud with an external shrouding gas was used to plasma spray titanium powder feedstock with aim of reducing the oxide content in the as-sprayed coatings. The titanium coatings were assessed by optical microscope, scanning electron microscopy, X-ray diffraction, LECO combustion method and Vickers microhardness testing. The results showed that the presence of the shroud and the external shrouding gas led to a dense microstructure with a low porosity in the plasma-sprayed titanium coatings. The oxygen and nitrogen contents in the titanium coating were kept at a low level due to the shielding effect of the shroud attachment and the external shrouding gas. The dominant phase in the shrouded titanium coatings was mainly composed of α-Ti phase, which was very similar to the titanium feedstock powders. The shrouded plasma-sprayed titanium coatings had a Vickers microhardness of 404.2 ± 103.2 HV

Experimental investigation of the elastoplastic response of aluminum silicate spray dried powder during cold compaction

Mechanical experiments have been designed and performed to investigate the elasto-plastic behaviour of green bodies formed from an aluminum silicate spray dried powder used for tiles production. Experiments have been executed on samples obtained from cold compaction into a cylindrical mould and include: uniaxial strain, equi-biaxial flexure and high-pressure triaxial compression/extension tests. Two types of powders have been used to realize the green body samples, differing in the values of water content, which have been taken equal to those usually employed in the industrial forming of traditional ceramics. Yielding of the green body during compaction has been characterized in terms of yield surface shape, failure envelope, and evolution of cohesion and void ratio with the forming pressure, confirming the validity of previously proposed constitutive models for dense materials obtained through cold compaction of granulates.Comment: 17 pages; Journal of the European Ceramic Society, 201

Atomization and mixing study

The state of the art in atomization and mixing for triplet, pentad, and coaxial injectors is described. Injectors that are applicable for LOX/hydrocarbon propellants and main chamber and fuel rich preburner/gas generator mixture ratios are of special interest. Various applicable correlating equations and parameters as well as test data found in the literature are presented. The validity, utility, and important aspects of these data and correlations are discussed and the measurement techniques used are evaluated. Propellant mixing tests performed are described and summarized, results are reported, and tentative conclusions are included