Pretreatment of citrus by-products affects polyphenol recovery:a review

A large amount of citrus waste is generated annually. This waste is of great economic worth, since it contains high levels of polyphenols, which have attracted scientific interest due to their potent antimicrobial and antiradical activities. Pretreatment is a crucial step that precedes the extraction process and influences the yields and quality of polyphenols. This review emphasizes the effect of different drying processes, such as freeze drying, hot-air drying, vacuum drying, microwave drying, infrared drying, and high-speed drying, on the polyphenol retention in citrus by-products. Further treatments of the dried citrus by-products for assisting the liberation of bound polyphenols are also provided and comprehensively discussed

Dimensional change of wool fabrics in the process of a tumble-drying cycle

The file attached to this record is the author's final peer reviewed version. The Publisher's final version can be found by following the DOI link.Currently domestic tumble dryers are popularly used for drying garments; however, excessive drying and the inappropriate way of tumble agitation could waste energy and cause damage to or the dimensional change of garments. Shrinkage of wool fabrics during tumble drying causes a serious problem for wool garments. The current study investigated the shrinkage of untreated and Chlorine-Hercosett–finished wool fabrics at different drying times. Temperature of air in the tumble dryer, temperature of fabric, moisture content of fabric, and dimensional change at different drying times were measured. For the duration of the tumble drying, the rise of fabric temperature and the reduction of moisture content on the wool fabric were investigated to explore their relationship to the shrinkage of wool fabrics in the tumble-drying cycle. It was found that the tumble-drying process can be divided into different stages according to the temperature change trend of wool fabrics. The shrinkage mechanisms of the untreated and the treated fabrics were different. The dimensional change of untreated wool fabric was caused mainly by felting shrinkage during tumble drying. Chlorine-Hercosett–finished wool fabric can withstand the tumble-drying process without noticeable felting shrinkage due to the surface modification and resin coating of surface scales of wool fibers. The finding from the current research provides further understanding of the shrinkage behavior of wool fabrics during the tumble-drying process, leading to optimizing operational parameters at specific stages of a tumble-drying cycle

The effects of drying methods and storage conditions on pea seed (Pisum sativum L.) quality and the relationship between high temperature drying and maize seed (Zea mays L.) stress cracks : this thesis presented in fulfilment of the requirements for the degree of Master of Applied Science (Agricultural Engineering) in the Institute of Technology and Engineering, Massey University, New Zealand

High temperature and high relative humidity adversely affect the quality of seeds, and are features of tropical climate. Seed drying and storage are being used increasingly in developing countries to improve seed storage and quality. This study was undertaken to evaluate a range of seed drying methods and storage conditions with the view to selecting an appropriate method(s) for use in tropical countries. Pea (Pisum sativum L.) seeds at three initial seed moisture content (m.c.) of 23.8, 18.0 and 14.5% were dried to 10% seed m.c. before storage. The performances of four different drying methods: artificial dryer (Kiwi Mini) set at 30°C or 45°C, natural sun drying, and in-bin natural ventilation drying were evaluated. Natural sun drying, and in-bin natural ventilation drying were conducted from March to May, 1997, when mean temperature and relative humidity during sunny days were 17°C and 60% respectively. The dried seeds were stored under two conditions: open storage at 20.5°0 and 55% relative humidity (r.h.), and closed storage at 25°C and 90% r.h. for 20, 40, and 60 days. Time and energy consumed for drying by the different methods were determined to compare the drying efficiency when combined with quality of the seed. Deterioration of the seed due to storage conditions and drying methods used was determined by assessing their effects on seed germination, abnormal seedlings, dead seed, hollow heart percentages, and conductivity. Seed samples dried by the Kiwi Mini dryer set at 45°C took 7 hours and those set at 30°C took 17 hours. It took 54 hours with natural in-bin ventilation drying, while sun drying took 37 hours. However, energy consumed when drying seeds at 30°C was 17 kWh, which was more than twice that at 45°C. Seed germination was not significantly different between drying methods, but averaged only 75% because of sprouting damage of the crop prior to harvest. Germinations after open and closed storage for 20 days did not differ, although some differences appeared after 40 days of storage. However, open and closed storage for 60 days significantly reduced seed germination to 54 and 33% respectively. Because seeds are heat-sensitive, drying air temperature and drying rate are particularly important to avoid internal seed breakage, cracking and splitting, fungal growth, and loss of germination and vigour. Selected studies have shown that seed can be dried at high temperature for a short time, followed by tempering to re-distribute moisture and temperature inside the seed, thus reducing the percentage of cracking. Thus, a second experiment was conducted with maize (Zea mays L) to study the impact on seed viability of high temperature drying followed by tempering. Maize at 28.5% initial seed m.c. was dried at 60°C for short periods of 5, 10, 15, 20, or 25 minutes, followed by tempering for 45 minutes at either 30°C or 21°C. This cycle was repeated until maize seeds were dried to 13.0% m.c.. The percentage of cracked seeds, germination immediately after drying, and after an accelerated ageing test, did not differ between 30°C and 21°C tempering. Drying exposure times of up to 10 minutes per cycle at 60°C caused vertical cracks in up to 50% of seeds, but seed germination remained over 90% and seed vigour was also maintained. The percentage of seeds with stress cracks due to high temperature drying (5 - 25 minute cycles) at 60°C followed by tempering had polynomial relationships with seed germination and vigour. Seeds dried at the same temperature without tempering had their germination reduced from 99 to 20%

Modelling the primary drying step for the determination of the optimal dynamic heating pad temperature in a continuous pharmaceutical freeze-drying process for unit doses

In the pharmaceutical industry, traditional freeze-drying of unit doses is a batch-wise process associated with many disadvantages. To overcome these disadvantages and to guarantee a uniform product quality and high process efficiency, a continuous freeze-drying process is developed and evaluated. The main differences between the proposed continuous freeze-drying process and traditional freeze-drying can be found firstly in the freezing step during which the vials are rotated around their longitudinal axis (spin freezing), and secondly in the drying step during which the energy for sublimation and desorption is provided through the vial wall by conduction via an electrical heating pad. To obtain a more efficient drying process, the energy transfer has to be optimised without exceeding the product and process limits (e.g. cake collapse, choked flow). Therefore, a mechanistic model describing primary drying during continuous lyophilisation of unit doses based on conduction via heating pads was developed allowing the prediction of the optimal dynamic power input and temperature output of the electric heating pads. The model was verified by experimentally testing the optimal dynamic primary drying conditions calculated for a model formulation. The primary drying endpoint of the model formulation was determined via in-line NIR spectroscopy. This endpoint was then compared with the predicted model based endpoint. The mean ratio between the experimental and model based predicted drying time for six verification runs was 1.05 +/- 0.07, indicating a good accordance between the model and the experimental data

Assessment of Efficiency of Drying Grain Materials Using Microwave Heating

We present results of experimental work on studying the drying of a dense layer of grain using microwave heating. We investigated a series of techniques to supply heat to grain to assess energy efficiency of a microwave field. We studied the following ways of drying: a microwave method, a pulsating microwave method, a microwave-convective cyclic method with blow of a layer with heated air flow and air without preheating, simultaneous microwave-convective drying method.Studying the kinetics of drying in a microwave field showed that we can divide the process into heating periods (zero drying rate), constant (first drying rate) and falling (second drying rate). These periods are characteristic for drying of colloidal capillary-porous bodies at other methods of heat supply. We obtained empirical relationships for the drying rate and the average temperature of grain in the first period based on the generalization of experimental data on the study on drying of grain of buckwheat, barley, oats, and wheat. We presented kinetic dependences in a dimensionless form. They summarize data on the studied grains. The aim of comprehensive studies of various methods of heat supply during drying was determination of the optimal method and rational operational parameters, which ensure high intensity of the process and the required quality of the finished product with minimal energy consumption.All studies took place under identical conditions and for the same grain (oats) to ensure the accuracy of the comparison. We determined that the most preferable method is a simultaneous microwave-convective energy supply without air preheating, which minimizes specific energy consumption. Experimental studies on drying using a microwave field made possible to select the required process parameters: power, heating rate, mass, and form of loading. We plan to develop a technology for drying of grain using microwave energy based on the study dat

Model and simulation of a solar kiln with energy storage

A solar kiln with energy storage can be used for continuous drying. This kiln consisted of several units which were modeled to simulate it in operation. A model was proposed for each unit, and another based on laboratory tests for drying a wooden board by passing air across. These models were combined to produce a global model. Simulation results were then analyzed and showed that the use of storage was justified to reduce drying time. Moreover, with the judicious use of storage and air renewal, drying schedules could be produced for a better quality of dried wood

Advance Drying Technology for Heat Sensitive Products

This book presents the advance drying technology for heat sensitive products cited from international journals, handbooks, and current research of authors. In the first edition, the printing and publication was funded Diponegoro University. In this second edition, the publication was supported from Directory of Higher Education under competitive research grant. The topic discusses the current drying technology for heat sensitive product, challenges, development and application in accordance with high quality product as well as efficient energy usage. Unlike first edition, this book observes and evaluates several food products drying under air dehumidification. The conceptual process has been also submitted to Indonesian Patent 2014. In the first edition, the book consisted of 7 chapters. Whereas, in this second edition, the book was extended up to 10 chapters completed with application of air dehumidification for food drying. Chapter 1 discusses about the challenge and progress on drying technology development. Chapter 2 describes the application and research of vacuum and freezes dryer. It is followed by the concept of air dehumidified by zeolite for efficient drying, depicted in Chapter 3. Chapter 4 evaluates the conventional condenser and adsorption dryer for low temperature drying. Chapter 5 is an overview of microwave and radio frequency dryer. After that, Chapter 6 presents the types of dryers applied in industries involving tray, spray, fluidized, moving bed, and drum dryer. Chapter 7 evaluates the future possible development for innovative dryer namely adsorption dryer with zeolite for industry. Chapters 8, 9 and 10 present the application of air dehumidification for agriculture and food drying. These chapters are results of the research conducted during 2012 – 2014

DEVELOPMENT OF A NOVEL ENERGY EFFICIENT ADSORPTION DRYER WITH ZEOLITE FOR HEAT SENSITIVE PRODUCTS

Drying is a basic operation in wood, food, pharmaceutical and chemical industry. The operation is important to enhance the preservation properties of agriculture crops and pharmaceutical products, to reduce the costs for transportation, to increase consumer convenience of food products, and to obtain desired water content in raw material feed for next unit process in industry. Currently several drying methods are used, ranging from traditional to modern processing: e.g. direct sun drying, convective drying, microwave and infra-red drying, freeze and vacuum drying. However, the current drying technology is often not efficient in terms of energy consumption (energy efficiency of 20-60%) and has a high environmental impact due to combustion of fossil fuel or wood as energy source. This work discusses on the development of adsorption drying with zeolite to improve the energy efficiency as well as product quality. In this process, air as drying medium is dehumidified by zeolite. As a result humidity of air can be reduced up to 0.1 ppm. So, for heat sensitive products, the drying process can be performed in low or medium temperature with high driving force. The study has been conducted in three steps: designing the dryer, performing laboratory scale equipment (tray, spray, and fluidised bed dryers with zeolite), and evaluating the dryer performance based on energy efficiency and product quality. Results showed that the energy efficiency of drying process can reach 70-80% in which is 15-20% higher than that of conventional dryer. Index Term— adsorption, drying, energy efficiency, zeolite, heat sensitiv