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Synthesis of Five‑, Six‑, and Seven-Membered 1,3- and 1,4-Heterocyclic Compounds via Intramolecular Hydroalkoxylation/Hydrothioalkoxylation of Alkenols/Thioalkenols

By Manash J. Deka (1608136), Kiran Indukuri (1608133), Sabera Sultana (1608142), Madhurjya Borah (1608145) and Anil K. Saikia (1608139)

Abstract

Intramolecular hydroalkoxylation/hydrothioalkoxylation of nitrogen-tethered alkenes and alcohols/thiols mediated by boron trifluoride etherate leads to five-membered thiazolidine, six-membered 1,4-oxazines (morpholines) and tetrahydro-2<i>H</i>-1,4-thiazines (thiomorpholines), and seven-membered 1,4-oxazepanes in good yields

Topics: Biochemistry, Genetics, Pharmacology, Science Policy, Mental Health, Infectious Diseases, Virology, Chemical Sciences not elsewhere classified, hydroalkoxylation, thiazolidine, oxazepane, oxazine, Compound, Synthesi, alkene, tetrahydro, Heterocyclic, thiomorpholine, Alkenol, boron trifluoride etherate, yield, Hydroalkoxylation, morpholine, Intramolecular
Year: 2015
DOI identifier: 10.1021/acs.joc.5b00049.s004
OAI identifier: oai:figshare.com:article/2170522
Provided by: FigShare
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