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暂态电化学表面增强拉曼光谱研究对硝基苯硫酚分子的电化学还原过程
Authors
凌云
刘国坤
宗铖
汤儆
Publication date
28 December 2019
Publisher
Doi
Cite
Abstract
对硝基苯硫酚是表面增强拉曼光谱研究中最常用的探针分子之一,对硝基苯硫酚在电极表面电化学还原反应的研究有助于对芳香族硝基化合物还原机理的认识.本文应用暂态电化学-表面增强拉曼光谱技术,研究了对硝基苯硫酚在循环伏安和计时电流法过程中的表面增强拉曼光谱.结果表明,实验实现了完全与电化学检测时间分辨率同步的表面增强拉曼光谱检测,以最快5毫秒的时间分辨率研究了对硝基苯硫酚分子在金电极表面的还原过程.结果分析推测其此反应过程极快,在5毫秒的时间分辨率下仍难以捕获其中间物种.本研究为人们更深层次研究和认识硝基苯类化合物电化学还原过程提供了参考和方向
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Last time updated on 20/11/2020