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EBSD characterisation of Y<inf>2</inf>Ba<inf>4</inf>CuUO<inf>x</inf> phase in melttextured YBCO with addition of depleted uranium oxide
Authors
,
DA Cardwell
+4 more
N Hari Babu
MR Koblischka
A Koblischka-Veneva
F Mücklich
Publication date
1 June 2006
Publisher
Abstract
Melt-textured YBCO samples processed with added Y2O3 and depleted uranium oxide (DU) contain nano-particles, which have been identified previously as Y2Ba4CuUOx (U-411). This phase has a cubic unit cell, which is clearly distinct from the orthorhombic Y-123 and Y-211 phases within the YBCO system. In samples with a high amount of DU addition (0.8 wt-% DU), U-2411 particles have sizes between 200 nm and several νm, so identification of the Kikuchi patterns of this phase becomes possible. Together with a parallel EDX analysis, the particles embedded in the Y-123 matrix can be identified unambiguously. In this way, a three-phase EBSD scan becomes possible, allowing also the identification of nanometre-sized particles in the sample microstructure. © 2006 IOP Publishing Ltd
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CUED - Cambridge University Engineering Department
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Last time updated on 15/07/2020