Kaolin and bauxite were used as alumina and silica sources to synthesize zeolites hydrothermally. The source mate-rials as well as the synthesized zeolites were characterized by X-ray diffraction (XRD) scanning electron microscopy (SEM), en-ergy dispersive x-ray analysis (EDX) and Fourier transformed infrared spectroscopy (FTIR). XRD spectra of the bauxite showed Gibbsite phase whereas that of kaolin gave 32.4 % quartz and 67.6 %. The main phases of zeolites obtained after hydrothermal crystallizations were zeolite types LTA, analcime and zeolite X. Longer crystallization time resulted in phase change of the zeo-lites into sodalite. Hence, natural raw materials such as bauxite and kaolin have the attractive features of providing the staring reagents for the synthesis of ultrapure synthetic zeolites
