Synthesis, crystal structure and study of X-H…A interactions in<b style=""> </b>N,N′-bis-(4-methoxy-benzylidine)-hydrazine

Abstract

602-605Synthesis and crystal structure of N,N′-bis-(4-methoxy-benzylidine)-hydrazine have been reported in this paper. The title compound crystallizes in the monoclinic space group C2/c with unit cell parameters a = 17.416(3), b = 10.711(3) and c =8.428(3)Å, =113.64(2)o, V = 1440.2(8)Å3 and Z = 4. The structure has been refined to a R-value of 0.038 for 937 observed reflections. The molecules adopt columnar packing in the unit cell and the crystal structure is stabilized by two intra- and five intermolecular hydrogen bonded interactions