Data to support study of coordination polymers of hexakis(isonicotinoyl)cyclotricatechylene (L) including those of [M3L2] composition with M = Re, Co, Cu or N

Berry, Gilberte Therese

Boyadjieva, Sophia

Hardie, Michaele

Oldknow, Samuel

Thorp-Greenwood, Flora

English

Research Data Leeds Repository (University of Leeds)

Summary of data/filesCompound identificationL1 = (±)-2,3,7,8,12,13-Hexa(pyridyl-4-carboxylate)-10,15-dihydro-5H-tribenzo[a,d,g]cyclononene (trivial name = hexakis(isonicotinoyl)cyclotricatechylene)Compound 1 = [Re3(L1)2Br3(CO)3]∙n(CH3NO2)∙m(H2O)Complex 2a = [Co3(H2O)6(L1)2]∙6(NO3)∙n(dimethylformamide)  Complex 2b = [Cu3(H2O)6(L1)2]∙6(NO3)∙n(dimethylformamide)  Complex 2c = [Ni3(H2O)6(L1)2]∙6(NO3)∙n(dimethylformamide)  Complex 3a = [Co3Cl6(L1)2]∙n(dimethylformamide)  Complex 3b = [Co3Br6(L1)2]∙n(dimethylformamide)  Complex 4 = [Co3I1.5(H2O)4.5L1)2]∙4.5I∙m(dimethylformamide) Complex 5 = [Cu2(L1)(trifluoroacetate)3(isonicotinate)]∙n(dimethylformamide) Complex 6 = [Ag2(L1)(dimethylformamide)2]∙2BF4∙2(H2O)∙6(dimethylformamide) NMR.zipImages (*.PDF) and raw data for Nuclear Magnetic Resonance Data of L1 indimethylsulfoxide (DMSO) solutionCrystal.zipData for single crystal structure determinationsEach folder contains: X-Ray data file as name.hkl Original data file where SQUEEZE procedure has been used if appropriate Final refinement results as name.res Crystallographic information file as name.cif Structure factor file as name.fcfAnalysis.zipAdditional characterisation data of compounds including: Mass spectrum of L1 Infrared spectroscopy of all compounds (Infrared.pdf) Thermogravimetric Analysis Data (TGA data.pdf) CHN Elemental analysis resultsSEM-EDX.zipData and images for energy dispersive X-ray spectroscopy

Data to support study "2D networks of metallo-capsules and other coordination polymers from a hexapodal ligand"

http://archive.researchdata.leeds.ac.uk/378/1/readme.pdf

Data to support study "2D networks of metallo-capsules and other coordination polymers from a hexapodal ligand"

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Research Data Leeds Repository (University of Leeds)