In this work nanowires (Co, Ni and Fe) were obtained via template synthesis, using etched track polymer matrix. The peculiarity of electrodeposition of Co and Ni was investigated and discussed: When filling
the pores of a small diameter (0.1 and 0.2 microns) the dependence of current on time passes through a
minimum. It can be supposed that the difficulties, appearing while filling nanosized pores, are related to
the peculiarities of diffusion in narrow channels. The electrolyte for Fe deposition into nanosized pores was
selected, the necessity of agitation was demonstrated. The results of X-rays analysis demonstrate that obtained wires have polycrystalline structure, which slightly depends on the deposition voltage. Mossbauer
spectroscopy was used for investigation of Fe samples. The obtained sextet corresponds to α-Fe with polycrystalline structure. Two types of Fe atoms were found. The presence of two types of oxides was also detected.
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