Objective of this paper is synthesis of metal-oxide supported on conducting substrate by electrochemical deposition. According to this study analysis of metal oxide thin film were done for physico-chemical properties like pH, current density, specific capacitance Vs voltage, surface area, cycle stability and coulombic efficiency. In order to get efficient metal-oxide thin film for various metal-oxide. Finally, higher energy density materials with better stability in an actual operating condition can be obtained by chemical route