This study focuses on preparing Antimony Nanoparticle Multi-walled Carbon (ANMWC) composite as an effective adsorbent and then the effect of produced composite in BPA removal from aqueous solutions was studied. ANMWC were prepared using chemical method and characterized with X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR) and Brunauer-Emmett-Teller (BET). Moreover, the removal efficiency of prepared AMWCNT and Nanoparticle Multi-walled Carbon (MWCNT) in removal of Bisphenol A was investigated. Results revealed that the BPA removal efficiency by AMWCNT increased from 80 to 93 with the increase of contact time 5 to 60 min. The maximum removal efficiency for the both adsorbents was seen at pH 7, which was 85 for MWCNT and 95 for ANMWC composite. According to the results obtained, pHzpc for both adsorbents was 7. Results showed that the adsorption process followed the pseudo-first order model with a high correlation value and BPA adsorption on MWCNT followed the Langmuir isotherm model
