This thesis deals with chosen aspects of terahertz (THz) technology that have potential in defense and security-related applications. A novel method for simultaneous data acquisition in time-resolved THz spectroscopy experiments is developed. This technique is demonstrated by extracting the sheet conductivity of photoexcited charge carriers in semi-insulating gallium arsenide. Comparison with results obtained using a standard data acquisition scheme shows that the new method minimizes errors originating from fluctuations in the laser system out-put and timing errors in the THz pulse detection. Furthermore, a new organic material, BNA, is proved to be a strong and broadband THz emitter which enables spectroscopy with a bandwidth twice as large as conventional spectroscopy in the field. To access electric fields allowing exploration of THz nonlinear phenomena, field enhancement properties of tapered parallel plate waveguide
