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First example of organonickel complex bearing three cyclic substituents in the σ-bonded aromatic ring: Bromo[(2,2' -bipyridine)-2,4,6-tricyclohexylphenylnickel]
Authors
Babaev V.
Dobrynin A.
+7 more
Gafurov Z.
Khayarov K.
Krivolapov D.
Rizvanov I.
Sakhapov I.
Sinyashin O.
Yakhvarov D.
Publication date
1 January 2016
Publisher
Abstract
© 2016 Mendeleev Communications. Published by ELSEVIER B.V.The electrochemical reduction of [NiBr2(bpy)] (bpy is 2,2'-bipyridine) complex in the presence of 2,4,6-tricyclohexylphenylbromide (TchpBr) in undivided electrochemical cell supplied with a sacrificial nickel anode results in the one-pot formation of an organonickel complex [NiBr(Tchp)(bpy)] bearing three cyclic substituents in the s-bonded aromatic ring. The synthesized complex was characterized by various methods including single crystal X-ray analysis
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Last time updated on 07/05/2019