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Dynamic NMR study of cyclic derivatives of pyridoxine
Authors
Galiullina L.
Garipov M.
+4 more
Klochkov V.
Rakhmatullin I.
Shtyrlin Y.
Strel'nik A.
Publication date
1 January 2014
Publisher
Abstract
A series of pyridoxine derivatives was investigated by 1H and 2D nuclear overhauser enhancement spectroscopy (NOESY) NMR. The free energies of activation for the pyridyl-oxygen rotation of the 2,4-dinitrophenyl ether of the seven-membered acetals of pyridoxine were measured by dynamic NMR. A conformational exchange between the chair and twist forms of the seven-membered acetal ring was confirmed by dynamic NMR and STO3G computations. © 2014 John Wiley & Sons, Ltd
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Last time updated on 07/05/2019