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β-Keto phosphonic esters - Communication 11. Action of diazomethane on diethyl acetyl- and benzoylphosphonates
Authors
Arbuzov B.
Polezhaeva N.
Shamsutdinova A.
Vinogradova V.
Publication date
1 January 1963
Publisher
Abstract
1. By the reaction of diazomethane with diethyl acetylphosphonate diethyl 1,2-epoxy-1-methylethylphosphonate and a little diethyl acetonylphosphonate were obtained. 2. Diethyl 1,2-epoxy-1-methylethylphosphonate was obtained also by the oxidation of diethyl isopropenyl-phosphonate with peroxyacetic acid. 3. By the reaction of diazomethane with diethyl benzoylphosphonate diethyl phenacylphosphonate was obtained. 4. The addition of phosphorus pentachloride to α-ethoxystyrene gave β-ethoxystyrylphosphonic dichloride, which was converted into diethyl β-ethoxystyrylphosphonate. Hydrolysis of the latter gave diethyl phenacylphosphonate. © 1964 Consultants Bureau Enterprises, Inc
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Last time updated on 07/05/2019