Synthesis of <i>gem</i>-Difluorinated Nitroso
Compounds
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Abstract
A method for the
synthesis of <i>gem</i>-difluorinated
nitroso compounds is described. The reaction involves interaction
of organozinc reagents with (bromodifluoromethyl)trimethylsilane
followed by nitrosation of difluorinated organozinc species with an <i>n</i>-butyl nitrite/chlorotrimethylsilane system
