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ZnF2包覆对锂离子电池正极材料LiNi0.5Mn1.5O4性能的影响
Authors
张灵志
李延伟
+3 more
杨建文
谢迪志
陈权启
Publication date
1 January 2017
Publisher
Abstract
采用溶胶-凝胶法制备了LiNi0.5Mn1.5O4正极材料,并利用Zn F2对其表面进行包覆改性。XRD、SEM和TEM测试表明,包覆处理不影响材料的晶体结构,2%(质量分数,以LiNi0.5Mn1.5O4质量计,下同)的Zn F2在LiNi0.5Mn1.5O4表面形成了约7 nm厚均匀包覆层。对未包覆的LiNi0.5Mn1.5O4和1%、2%、3%的Zn F2包覆后的LiNi0.5Mn1.5O4的电化学性能进行了考察,发现Zn F2包覆能够减弱电解液与LiNi0.5Mn1.5O4正极材料之间的相互作用,稳定电极表面,提高材料的电化学性能。其中,2%Zn F2包覆样品表现出最佳的循环性能和倍率性能,0.2C电流倍率下循环200圈后,其放电比容量维持在109.0 m A·h/g,保持率为79.7%;5 C电流倍率下循环500圈后,放电比容量维持在94.2 m A·h/g,保持率为85.6%
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Last time updated on 04/12/2021