CORE
🇺🇦
make metadata, not war
Services
Services overview
Explore all CORE services
Access to raw data
API
Dataset
FastSync
Content discovery
Recommender
Discovery
OAI identifiers
OAI Resolver
Managing content
Dashboard
Bespoke contracts
Consultancy services
Support us
Support us
Membership
Sponsorship
Community governance
Advisory Board
Board of supporters
Research network
About
About us
Our mission
Team
Blog
FAQs
Contact us
Reaction of some 2-quinolone derivatives with phosphoryl chloride: Synthesis of novel phosphoric acid esters of 4-hydroxy-2-quinolone
Authors
Ahvale
Bell
+26 more
Blankenstein
Boulos
Capps
de Arce
Huffman
Irwing
Jung
Kafka
Klásek
Klásek
Leach
Lutz
Malle
Matsubara
Mislow
Nasr
Patel
Pomeisl
Sokrates
Stadlbauer
Stadlbauer
Stadlbauer
Stadlbauer
Stadlbauer
Steinschifter
Tagawa
Publication date
22 May 2013
Publisher
'Wiley'
Doi
Abstract
3-Chloroquinoline-2,4-diones do not react with phosphoryl chloride, however, 2,4-dichloroquinolines and/or 4-chloroquinolin-2-ones are formed in the presence of N,N-dimethylaniline. Along with these compounds, small quantities of novel dihydrogen phosphates of 4-hydroxyquinolin-2-ones were isolated. We outline a simple procedure that allows for the preparation of these compounds in moderate to good yields. All compounds were characterized by 1H and 13C NMR, IR, EI-MS, and ESI-MS spectroscopy, and in select cases by 31P NMR spectroscopy. © 2013 HeteroCorporation
Similar works
Full text
Available Versions
Institutional repository of Tomas Bata University Library
See this paper in CORE
Go to the repository landing page
Download from data provider
oai:publikace.k.utb.cz:10563/1...
Last time updated on 15/05/2014
Crossref
See this paper in CORE
Go to the repository landing page
Download from data provider
Last time updated on 05/06/2019