Molkentin, Joachim

Precht, D.

English

OA OpenAgrar repository

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' ' A -"' -' ' .-' "" •c---' 9 ' "' -;,.. . -· -12 ' A ~ .A --' 18 III „ 4 mean as mass 12 0 0 -- - III - "" -' l ' ' ' - - -- -. - -II ... 1 ' 0 3 6 9 0 0 -"" l ' • • ' . 1111 -12 18 '. ------' D 0 Ä IV D 0 A III • • A !III as mass mean 100 98'--~~~~~~~~~~~~J.._~-----~~~~~~~~~-l 102,.-~~~~~~--~~~~~-.-~~-------~~----~~~-100 98'---~~~~~~~~-~~~~.l...---~~~~~~~--~~~-l 102.---~~~~~-~~-~~~~~-,--~~--~~~~~--~~~~ 100 98'---~--~--~~~~~-~~~-L....~-~~~~~---~~~~~--l 102,-~~~~~~~~~--~~~--~~--~~~~~~~~---100 98'----~-~----~----~----~..I-..~~-·--·--~--~~~~~--' 102r-~~~~~--~~~~~---,--~~~-~~~~~~--~~-100 98'--~~~~~~~--~~~~..l-..--~~~~~~~~~~~....J 1()2.-------~~~~--~~~~~...,.---~--~~~~~------~-100 98~-~-~--~-~~~~~~~--"'--~~~~~--~--~~~~--l 102.--~~~~~--~~~~~~...,.-~~~~--~~~--~--~-100 98'--~~~~~~~~~~~~-'----~~~--~~~~---~--~....J 102,--~--~~~~---·---~~~-,----~--~~~----~~~--~ 100 98'--.!.-~-'--~-'-~--'-~---'~~-'--..!-....-'--~-'-~--i..~---''---~-'----'--l 3 6 9 12 18 24 3 6 9 12 18 24 annex no so 2 0 8 mass 2 3 4 6 8 0 2 3 4 6 8 10 y 0 11111 as 5 0 on an were summer were as 0. mean a a a a errors 1 1 = mass 8 1 (1)) use more runs no was ) were were 0 • 0 "' 2 was no reason as reasons can area reasons. as a annex were n was as as are mean as p s is as S= / is Cl mean x- -at s + (1 - a I -a f 2 a are one. p as: as sum errors can if F= zero. if 1 1 is no reason means were case errors are as as were mean as see mass 11 2) same were 1 1) 5 1 ensure a 12 use on 1 2 as 3 4 must a on (1 to l Screw cap with filter, against which the glass fibre and stafümary phase are pressed a to screw can .± ± ± ( 1 ,_ !;;/ ." ""'-, ~ "\ 2 \\ { ! - ~ 1111 1111 11 l 1 11 1 I \ 1 II 1\ )1 \1 ~\ '~ /!/ / to at a water one 4 1S at at c g cotton " to g 9 a H. 2 1 contents ;:)a11rm1e 3 6.76 8.92 8.95 11.53 1.58 0.88 5.65 1 5.65 74 76 9 Lab.2 Lab. 3 0 0 "' 0 1111 4 Lab. 5 Lab. 6 Lab. 7 Lab. 8 Lab. Lab. O \ 0 .240 + ..•...... + 01 LABOl LAB02 03 LAB03 04 LAB05 05 LAB08 I.AB09 07 LABlO iMEANSI .280 .320 .360 ..•••... + ...••.... + .•..•.... + ••••..•.. + .•.. ' .... + ..•••••.• + <-*-> <-*-·-> <:..*-> <--------*--------> <---*----> <---A---> <-*--> <----------*----------> <------------M------------> of f i mean mean rat of means td.dev. str thin- s Between- std. f of 95 ""' the mean L :7 35 33 in ·"' 7 25 p tes ) Bartlett test of mean va iefors test) test) of means s Sw rval ;... --- -~ means 2 .0206 is a st er .01722 is an outlier Not Normal None None 37.45 > 2.38 35;0.95) .301 .02801 . 1121 .02764 .301 0 +/- .02591 ;... ~ 1--v .. --10 01 LAB02 02 LAB03 03 LAB05 04 LAB08 05 LAB09 06 ALL MEANSI 0 .020 .030 .040 .050 .060 . 070 + ...... + ...•.. + ....•. + ...... + ...... +... . + ...... + ...... + ...... + ...... + <-------*------> <-------------*--------------> <-----*-----> <----------*----------> <-----A-----> <---------------M----------------> mean mean f means .of -1 Between-1 s f .95 con s 6 lett test) f mean values fors test} test) test) of means s ' mass 983 is a st er .0 53 is a st er Normal None None 22.66 > 2.53 30; (). 9:0) .04528 .01113 .00 3 .01 8 .0452 /- . 68 1 01 LABOl 02 LAB02 03 LAB03 04 LAB05 05 LAB06 06 LAB08 07 LAB09 08 LABl IALL MEANS I 0 .160 .200 7 6 1 1 .240 .280 .320 + ........ + .... , .. +.' '.' ... + •.....•. + ...... ' .+ ..... ' .+ ...... ' .+ ........ + <---*---> <--------*-------> <--*> <-------*-------> <------*------> <--*-> <---*----> <-----*-----> <---A---> <----------M---------·-> var mean mean F-rat o means str s Between-1 s et ances 3 r-8 6 4 2 2 of resul t) (Bartlet of tes test of means ....•• ~ 8···> ·-- ;.~""-~· -·--~-1 p N tes ) s >· . means 8 48 No outliers About None None t 36.29 > 2.25 40;0.95) .252 8 .03029 .012 2 .02987 .2 0 .. ~ + - .02532 10 ers 1 0 .480 .520 . 60 .600 .640 + •••..•.. + ....... + ......•. + ........ + ........ + ....... + ...•.... + .......• + 01 LABOl <--*-> 02 LAB02 <--------*--------> LAB03 <-*--» 04 I.Jl..B05 <---------*---------> i 05 LAB06 <-----*----> 06 LAB08 <-*-> 07 LAB09 <-----*------> 08 LABlO <------*-·------> IALL <----A-----> .MEANS ! <--------------M----------------> 1 means 8 4 tes ) outliers, no st ers Not ion of mean values Norma l e test) mean test) None l mean test None rat 54.67 > 2.25 ,40;0.95) Mean of means .58812 Std.dev. of means s .04 56 -1 ation Sw .01 77 . 4 18 of .95 .588 2 +/- .03475 66 63 T f l .6 57 ·-------·-- -·· 54 . cf-48 01 LABOl 02 LAB02 03 LAB03 04 LABOS 05 LAB06 06 LABOS 07 LAB09 08 LABlO IALL IMEANSI 1 L.;;Jvvv 1.1 1.1 0 1.1 1.000 1 1.100 1.200 1.300 + .. '., .. ,., .+. ' ........ +. '' .•••...• + ••.•...•.•. + .•. , •.• , •• + .........•. + <-*-> <--------*--------> <--*--> <-*> <--*---> <--*--> <-------*--------> <----A---> <------------M-----------> <---*----> 1 s p 0 ance ( of variances ett test) mean mean rat of means .dev.dr s l s Between-1 s of 1 1 test) test) of means ion s Sw Sb interval means 1. s~~·~··--,~--+------~----+~·--+------+-~----·~~-----1.--~~--i 01 LABOl 02 LAB02 03 LAB03 04 LAB05 05 LAB06 06 LAB08 07 LAB09 08 LABlO IALL !ME.ANS 1 4 0 2.150 2.250 2.350 2.450 2.550 2.650 + ...... + .•..•. + .. ,., .+ ...... +.' .... + ..•..• + .. , ... + .... , .+ ...... + .. , .•. + <*-> <-----*-----> <-------*-------> <-*> <--*---> <-*-> !<--------*-------> <----A----> <---·------------M---------------> <--·*-> 1 1 2 0 .1 .1 5.200 5.400 5.600 5.800 6.000 01 LABOl <---*---> 02 LAB02 <--*--> 03 LAB03 <-*> 04 LAB OS <-·---*---> 05 LAB06 <--*----> 06 LA.BOB <*-> 07 LAB09 <----*---> 08 LABlO <---------*--------> ALL <----A----> IMEANSI <---·-----------M-------------> f variance it 0 rat of means s Between-1 std. .95 i 6 t p tes Bartl t s va test test} test of means s rval 4 .10167 is an outlier Not Normal None None 96.27 > 2.25 5. 396 .19936 .0 977 .19832 5.64396 +/- .16667 I T 1 ' 10 01 LABOl 02 LAB02 03 LAB03 04 LAB05 05 LAB06 06 LAB08 07 LAB09 OB LABlO IALL !MEA.l\JS 1 0 9.900 1 1 .1 .100 .11 .1 .1 10.300 111 10.500 10.7 10.900 ..... + ...•.. + .•..• + •.•.. + ...... + ....• + ...... + ....• + ••..• + .••.•. + ••••• + <----*-----> <----*-----> <*> <------*-------> <------*-----> <----*----> <---*---> <--------*-------> <---A---> <-----------M-----------> i Out mean 1 mean F-rat Mean of means S .dev. st W.i l s Between- std. f 0.95 1 9 1 7 5 1 3 1 1 2 f re ts p cates N test) Bartlett test) of mean va f ors test test) tes ) ion f means at ···-···· ~ _. .. .-. -- - .. ;_.--.„ ...•...... v ' 1 s Sw ···-, ...... .... 8 4 outliers, st ers Normal None None 39.44 > 2.25 1 . 4 69 7 .22221 .08668 .21938 10.46917 - .18577 - .. ... . , ... . ... ~ " 10 01 LABOl 02 LAB02 03 LAB03 04 LAB05 05 LAB06 06 LAB08 07 LAB09 08 LAB10 ALL MEANS 0 11.900 7 7 .1 12.100 113 .1 12.300 12.500 12.700 12.900 + ...... + .... '.+ .. ' ... +.' .... + ...... + .•.... + ...... + .....• + ...... + .•..•• + <-*-> <---*----> <-*-> <----*---> <------*------> <---*----> <----*----> <--------*--------> <----A----> <--------------M--------------> of of mean lues 1 mean F-rat o means s f st l s Between--1 of 1 3 8 6 1 .4 1 .2 2 114 icate N tes (Bartlett tes ) o mean values fors test) test test) of rneans s Sw Sb u means 8 48 No outl s ers Normal None None 75.73 > 2.25 ,40;0.9S) 12.52521 .2535 .07 38 .25190 12.52521 + .212 0 1 01 LABOl 02 LAB02 03 LAB03 04 LAB05 05 LAB06 06 LA.BOB LAB09 OB LABlO IALL !MEANSI 1 1 1 1 1 0 1 9.700 15 9.900 10.100 10.300 + ........... + ...•..•... + •..•....... + ........... + ••.. '.'' •. +.' ....... ' .+ <-*-> <------*-------> <--------*-------> <--*--> <-------*-------> <--*-----> <--·---* ---·---> <-----*------> <-----A----> <----------------M----------------> 0 i l std. Between- s 0 0.95 116 resu1ts p N lett test) t _.es te t of means 1 s s Sw Sb l means 8 8 No outliers no s ers Normal None None 6.86 > 2.25 ,10;0.'J';' 10.03 42 .17455 .04877 .17341 10. 3 2 +/- .14593 01 LABOl 02 LAB02 03 LAB03 04 LAB05 05 LAB08 06 LAB09 07 LABlO !ALL !MEANS! 1 7 1: 0 1 6.450 .550 6.650 6.750 6.850 + ........ + ... '' .. + ........ + ...... ' .+ .... , ... + ....... +, ••••••• + ........ + <-------*-------> <-*> <---*----> <*-> <------*------> <-----*----> <-----*----> <----A----> <---------------M---------------> 18 means f ca N 42 (Cochran No outliers, no s ers iances Bart ett test Not s Normal mean tes None mean test None E'-rat 68.49 > 2.38 Mean of means 6.69476 td.dev. f tr means s . 953 s Sw .02822 Between- Sb . 9463 f 0 0. i rval 6.69 76 + - .08817 f the mean 10 1: 01 LABOl 02 LAB02 03 LAB03 04 LAB OS LAB08 06 LAB09 07 LABlO IALL !MEANS 119 0 1 9 5.850 5.950 .050 6.150 6.250 + ........ + .•..... +., ...... + ........ + ...•........... + ........ + ........ + <----*---> <-----*------> <-*--> <*> <------*-------> <--*---> <------*------> <---A----> <------------M------------> 1 an ts p 7 f N 42 test) No outliers, no s ers i (Bart tt test) Not of mean Normal test) mean test) None l mean test) None rat 49.15 > 2.38 Mean f means 6.11429 .of distribution f means s . 7964 Sw .02783 Sb .07883 of .11429 +/- .o 365 -~ -~ - - -' ' --~ --6 ~ ' 10 mass 0 6. 01 LABOl 02 LAB02 03 LAB03 04 LAB05 05 LAB08 06 LAB09 07 LABlO IALL MEANSi 6 7 6.800 1 6.900 7.000 + ........... + .......... + ...................... + .......... + ........... + <--*---> <-*-> <---------*--------> <-------*-------> <---*---> <---------*---------> <----A-----> <---------------M----------------> f i l mean l mean E'-rat Mean of means .dev.of 1 s Between-1 1 s N test (Bartlett test of mean values iefors test lues (Nal test test str of means s Sw std. ation 0.95 1 7 " '"'' -9 - -" -8 _,_ -~ -7 means 7 42 No outliers, no st ers About Normal None None 48.37 > 2.38 6.86381 . 7684 .02706 .07604 6.86381 + - .07106 -,,, "'""''" '"'" '"'"""" ->-' --~- ---~-5 10 1 0 8.400 8.600 8.800 9.000 + ........... + ....•.•..• , ..•..•..•. + ........... + .......... + ....•...... + 01 L.ABOl <-*> 02 L.AB02 <---------*--------> 03 LAB03 <*> 04 LAB05 <-----*-----> 05 .LAB06 <-----*----> 06 LAB08 <--*--> 07 LAB09 <---*--> 08 LAB10 <--------*--------> ALL <-----A----> ME.ANS 1 <----------------M---------------> f i Outl mean Outl mean va F-rat Mean f .means Std.dev. f l Between- s f 0.95 t p N tes Bart test) mean va test) test) tes ) of means 1 s Sw 8 8 No iers, no ers Not Normal None None 79.95 > 2.25 , '10;0. 8.68833 .17122 .04690 .17014 8.68833 +/- .14314 -- --· -·---0 mass 1 1 11 11 11.1 11.1 11 0 11 .11 .1 10.900 11.100 .300 11. 500 11. 700 11. 900 12.100 + ..••. +.,, •• + .• ' .•.. , .+. ' ... + ..... + ... ' .+., ... + .... +.' ... + ..... + ..... + 01 LABOl <--*-->! 02 LAB02 <--*·--> 03 LAB03 <*> LA:S05 <----*---> 05 LAB06 <----*---> 06 LAB08 <--*-·-> 07 LAB09 <--*--> 08 LABlO <-------*------> AI,L <---A----> ME.ANSI <------------M-------------> 0 f 1 l mean Mean of means Std.dev.o s thin-1 s Between-1 1 s p es test Bartlett test) f mean values lliefors test) test ion of means s at Sw a Sb of 0.95 con l 8 48 .11929 s a s er About Normal 11.996 s an outlier None 1 7.41 > 2.25 ' ,40;0.95111.4016 .27610 .06526 .27 81 1 . 4 167 + .23 83 10 LABOl LAB02 LAB03 IAB05 LAB06 06 LAB08 LAB09 08 LABlO MEANS 0 10.600 7 7 .1 7 .1 11. 000 1 11. 400 .800 ..••..•.•.. + ......•... + .......•... + ....•...... + .......... + ........... + <-·---*-----> <*··> <--*--> <-----*--·--> <-------*-------> <----A----> --> <-------------M-------------> <--*---> f f out liers no st ers let tes Not s test) 11.6 83 is an li r mean s test) 11. 6 833 is a s er F-rat 85.97 > 2.25 Mean of means 10.96083 Std.dev.of str of means s .28992 s . 765 Between- Sb .28822 . 5 l 10.9 83 +/- .24238 I 1 3 1 .1 5. 5.900 .•...... + ....... + ................ + ....... . <--*---> <-----*-----> <------*------> <-----------*-----------> <---A---·> .100 .300 . ..•.... + ........ + <------ --> <------*-----·-> <----------M-----------> means ets f icates 4 tes . 27 is a st er s Norma 6 -~ ---- --- ---- -- T - 1 ---1 1 1 1 1 10 

The certification of the triglyceride contents of an anhydrous butter fat reference material with additional value for free cholesterol - CRM 519

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The certification of the triglyceride contents of an anhydrous butter fat reference material with additional value for free cholesterol - CRM 519

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