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新型含氟季铵盐(C_4H_9)_4NAlF_4的合成、表征及电化学性质
Authors
周君
张懿
曹妍
李会泉
Publication date
1 January 2010
Publisher
Abstract
在氮气保护下,四丁基氢氧化铵水溶液与氟铝酸铵进行反应,采用二氯甲烷萃取分离和异丙醇共沸除水方法对反应产物进行处理,制备了高纯的新型含氟季铵盐-四丁基铵的四氟铝酸盐,对其结构进行了表征,并对其物理及电化学性质进行了研究.结果表明,该季铵盐的熔点为204℃,400℃时分解,220℃时的电导率为4.67S/m,电化学窗口为4.7V,具有熔点低、电导率高、热稳定性和电化学稳定性好等优点,是一种很有潜力的低温电解质
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Last time updated on 09/11/2016