OLIVEIRA, R. C.

QUEIROZ, S. C. do N. de

RATH, S.

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164 | Congresso Latino Americano de Cromatograa e Técnicas Relacionadas – COLACRO XIV| C164 |02 de Outubro (3a feira) Cromatograa – Espectrometria de MassasMS(MS) | GC-MS(MS) | LC-MS(MS)DESENVOLVIMENTO E VALIDAÇÃO DE MÉTODO MULTIRRESÍDUOS PARA DETERMINAÇÃO DE RESÍDUOS DE AGROTÓXICOS EM PÓLEN APÍCOLA POR GC-MS/MS ION TRAP.Renata Cabrera de Oliveira, Sônia Claudia do Nascimento Queiroz, Susanne Rath2SyOHQDStFRODWHPVLGRDSRQWDGRFRPRXPSRWHQFLDOELRLQGLFDGRUGDSUHVHQoDGHFRQWDPLQDQWHVDPELHQWDLVHPiUHDVQRVDUUHGRUHVGRVDSLiULRV3DUDDQiOLVHGHVVDVDPRVWUDVHPRQLWRUDPHQWRDPELHQWDO p QHFHVViULR GHVHQYROYHU PpWRGRV DQDOtWLFRV TXH DSUHVHQWHP VHOHWLYLGDGH HGHWHFWDELOLGDGH DGHTXDGDV2REMHWLYRGHVWH WUDEDOKR IRL GHVHQYROYHU H YDOLGDU XPPpWRGRDQDOtWLFRPXOWLUUHVtGXRVTXDQWLWDWLYRSDUDDGHWHUPLQDomRGHUHVtGXRVGHDJURWy[LFRVHPSyOHQDStFRODXWLOL]DQGRFURPDWRJUD¿DDJiVDFRSODGDjHVSHFWURPHWULDGHPDVVDVHPWDQGHPFRPDQDOLVDGRUGHPDVVDVGRWLSR,RQ7UDS$YDOLGDomRDQDOtWLFDIRLUHDOL]DGDGHDFRUGRFRPDVUHFRPHQGDo}HVGRGRFXPHQWR6$1&2GHWHUPLQDQGRIDL[DOLQHDUHOLQHDULGDGHH[DWLGmRSUHFLVmRVHOHWLYLGDGHHOLPLWHVGHGHWHFomRHTXDQWL¿FDomR2SUHSDURGHDPRVWUDIRLUHDOL]DGRSRUH[WUDomRVyOLGROtTXLGRFRPDFHWRQLWULOD$VHSDUDomRFURPDWRJUi¿FDIRLUHDOL]DGDHPFROXQDDQDOtWLFD5[L®6LOPP[PȝPXWLOL]DQGRJUDGLHQWHGHWHPSHUDWXUD$ DQiOLVH TXDQWLWDWLYD GRV DQDOLWRV $FHWRFORUR $ODFORUR $OGULQ %LRDOHWULQD 'LD]LQRQ'LVVXOIRWRQ (QGRVVXOIDQ DOID (WULQIyV )HPSURSDWULP )HQWRDWR )OXD]LIRSH +HSWDFORUR(Sy[LGR0DODWLRQ2[LÀXRUIHQ3DUDWLRQ(WLO3DUDWLRQ0HWLO3HQGLPHWDOLQD3LULPLIyV(WLO3URSDUJLWR 7HUEXIyV 7ULÀXUDOLQD H GR SDGUmR LQWHUQR /LQGDQR IRL UHDOL]DGD DWUDYpV GRPRQLWRUDPHQWRGRVVHXVtRQVSUHFXUVRUHV$VHOHWLYLGDGHGRPpWRGRDQDOtWLFRIRLYHUL¿FDGDSHODDXVrQFLDGHSLFRVLQWHUIHUHQWHVQRWHPSRGHUHWHQomRGRVDQDOLWRVHGRSDGUmRLQWHUQR2PpWRGRDSUHVHQWRXOLQHDULGDGHDGHTXDGDFRPFRH¿FLHQWHGHFRUUHODomRUPDLRUTXHSDUD DPDLRULD GRV DQDOLWRV$ SUHFLVmR GRPpWRGR IRL FRPSURYDGD DWUDYpV GRV YDORUHV GHGHVYLRSDGUmRUHODWLYRLQIHULRUHVDSDUDDPDLRULDGRVDQDOLWRVHPQtYHLVGHFRQFHQWUDomRDFLPDGHJNJ2VUHVXOWDGRVGHUHFXSHUDomRHQWUHHGHPRQVWUDUDPDH[DWLGmRGRPpWRGRDQDOtWLFR2VOLPLWHVGHGHWHFomR/2'SDUDRVDQDOLWRVDSUHVHQWDUDPYDORUHVHQWUHJNJHJNJ2VOLPLWHVGHTXDQWL¿FDomR/24¿FDUDPHQWUHJNJHJNJAgradecimentos)$3(63

Desenvolvimento e validação de método multirresíduos para determinação de resíduos de agrotóxicos em pólen apícola por GC-MS/MS ÍON TRAP.

RCAAP - Repositório Científico de Acesso Aberto de Portugal

http://www.alice.cnptia.embrapa.br/alice/bitstream/doc/952231/1/RAQueirozSCNXIVCOLACROp164.pdf

Desenvolvimento e validação de método multirresíduos para determinação de resíduos de agrotóxicos em pólen apícola por GC-MS/MS ÍON TRAP.

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