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The Journal of Organic Chemistry

Asymmetric Reduction of Electron-Rich Ketones with Tethered Ru(II)/TsDPEN Catalysts Using Formic Acid/Triethylamine or Aqueous Sodium Formate

Browne, P.L.

OpenGrey Repository

Lukacs's aesthetics and ontology, 1908-23

The asymmetric transfer hydrogenation (ATH) of ketones under aqueous conditions using tethered Ru(II)/η6-arene/diamine catalysts is described, as is the ATH of electron-rich substrates containing amine and methoxy groups on the aromatic rings. Although such substrates are traditionally challenging ones for ATH, the tethered catalysts work very efficiently. In the case of amino-substituted ketones, aqueous conditions give excellent results; however, for methoxy-substituted substrates, the more established formic acid/triethylamine system gives superior results

Soni, Rina

Hall, Thomas Howard

Mitchell, Benjamin P.

Owen, Matthew R.

Wills, Martin

Warwick Research Archives Portal Repository

Asymmetric reduction of electron-rich ketones with tethered ru(II)/TsDPEN catalysts using formic acid/triethylamine or aqueous sodium formate

The
asymmetric transfer hydrogenation (ATH) of ketones under aqueous
conditions using tethered Ru­(II)/η<sup>6</sup>-arene/diamine
catalysts is described, as is the ATH of electron-rich substrates
containing amine and methoxy groups on the aromatic rings. Although
such substrates are traditionally challenging ones for ATH, the tethered
catalysts work very efficiently. In the case of amino-substituted
ketones, aqueous conditions give excellent results; however, for methoxy-substituted
substrates, the more established formic acid/triethylamine system
gives superior results

Rina Soni (1301130)

Thomas H. Hall (1360713)

Benjamin P. Mitchell (1360716)

Matthew
R. Owen (1360710)

Martin Wills (1301133)

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Asymmetric Reduction
of Electron-Rich Ketones with
Tethered Ru(II)/TsDPEN Catalysts Using Formic Acid/Triethylamine or
Aqueous Sodium Formate

http://wrap.warwick.ac.uk/72787/1/WRAP_acs%252Ejoc%252E5b00990.pdf

Lukacs's aesthetics and ontology, 1908-23

Abstract

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Crossref

OpenGrey Repository

Warwick Research Archives Portal Repository

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