SIGLEAvailable at INIST (FR), Document Supply Service, under shelf-number : Y 30688 / INIST-CNRS - Institut de l'Information Scientifique et TechniqueFRFranc

Ashbrook, Sharon Elizabeth Marie

Bobkova, Irina E.

Chulanova, Elena A.

EaSTCHEM

Hua, Guoxiong

Irtegova, Irina G.

Konstantinova, Lidia S.

Nelyubina, Yulia V.

Rakitin, Oleg A.

Sanz Camacho, Paula

School of Chemistry

Slawin, Alexandra Martha Zoya

Vasilieva, Nadezhda V.

Woollins, John Derek

Zibarev, Andrey V.

OpenGrey Repository

Frontiers in low temperature plasma diagnostics  Les Houches, 23-27 January 1995

Synthesis of 3,4-disubstituted and fused 1,2,5-selenadiazolo[3,4-b]pyrazines via previously unknown 3,4-diamino-1,2,5-selenadiazole has been achieved in moderate to high yields. The compounds synthesized were characterized by elemental analysis, MS and multinuclear (1H, 13C and 77Se) NMR, and the structures of 3,4-diamino-1,2,5-selenadiazole, 5,6-dimethyl[1,2,5]selenadiazolo[3,4-b]pyrazine and 5-phenyl[1,2,5]selenadiazolo[3,4-b]pyrazine were confirmed by X-ray diffraction. Electrochemical reduction of 5,6-R2-1,2,5-selenadiazolo[3,4-b]pyrazines (R = Me, Ph) into persistent radical anions (RAs) was studied by cyclic voltammetry and the RAs were characterized by EPR spectroscopy combined with DFT calculation

Ashbrook, Sharon Elizabeth

Woollins, J Derek

University of St. Andrews - Pure

1,2,5-Selenadiazolo[3,4-b]pyrazines:synthesis from 3,4-Diamino-1,2,5-selenadiazole and Generation of Persistent Radical Anions

1,2,5-Selenadiazolo[3,4-b]pyrazines: synthesis from 3,4-Diamino-1,2,5-selenadiazole and Generation of Persistent Radical Anions (dataset)

Lidia S. Konstantinova

Irina E. Bobkova

Yulia V. Nelyubina

Elena A. Chulanova

Irina G. Irtegova

Nadezhda V. Vasilieva

Paula S. Camacho

Sharon E. Ashbrook

Guoxiong Hua

Alexandra M. Z. Slawin

J. Derek Woollins

Andrey V. Zibarev

Oleg A. Rakitin

Crossref

European Journal of Organic Chemistry

[1,2,5]Selenadiazolo[3,4-<i>b</i>]pyrazines: Synthesis from 3,4-Diamino-1,2,5-selena­diazole and Generation of Persistent Radical Anions

The authors acknowledge financial support from the Russian Foundation for Basic Research (Project 13-03-00072), the Presidium of the Russian Academy of Sciences (Programme No.8, Project 8.14) and the Leverhulme Trust (Project IN-2012-094). I.G.I, N.V.V., E.A.C. and A.V.Z. are grateful to the Ministry of Education and Science of the Russian Federation (Project of Joint Laboratories of Siberian Branch of the Russian Academy of Sciences and National Research Universities), and E.A.C. to the BP Company for postgraduate scholarship.Synthesis of 3,4-disubstituted and fused 1,2,5-selenadiazolo[3,4-b]pyrazines via previously unknown 3,4-diamino-1,2,5-selenadiazole has been achieved in moderate to high yields. The compounds synthesized were characterized by elemental analysis, MS and multinuclear (1H, 13C and 77Se) NMR, and the structures of 3,4-diamino-1,2,5-selenadiazole, 5,6-dimethyl[1,2,5]selenadiazolo[3,4-b]pyrazine and 5-phenyl[1,2,5]selenadiazolo[3,4-b]pyrazine were confirmed by X-ray diffraction. Electrochemical reduction of 5,6-R2-1,2,5-selenadiazolo[3,4-b]pyrazines (R = Me, Ph) into persistent radical anions (RAs) was studied by cyclic voltammetry and the RAs were characterized by EPR spectroscopy combined with DFT calculationsPeer reviewe

St Andrews Research Repository

English

1,2,5-Selenadiazolo[3,4-b]pyrazines : synthesis from 3,4-Diamino-1,2,5-selenadiazole and Generation of Persistent Radical Anions

https://research-repository.st-andrews.ac.uk/bitstream/10023/9198/1/Woollins_2015_EJOC_1_2_5_AM.pdf

Frontiers in low temperature plasma diagnostics Les Houches, 23-27 January 1995

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University of St. Andrews - Pure

University of St. Andrews - Pure

University of St. Andrews - Pure

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St Andrews Research Repository

University of St. Andrews - Pure