应用改进固相合成法制备亚微米Li4Ti5O12锂离子电池材料.X射线衍射(XRD)、扫描电镜(SEM)和激光粒度分析分别显示:物相单一且粒度均匀,D50为0.886μm,属于亚微米级材料.合适的粒度和分布使得该材料展示出优良的电化学性能,以其装配的半电池中,0.1C首次放电容量为165 mAh/g,5C时放电容量可达107 mAh/g,10C时仍可达到54 mAh/g.The sub-micronmeteric Li4Ti5O12 powder material was successfully prepared through an improved solid-state synthesis process.The results of X-ray diffraction(XRD),scanning electron microscopy(SEM) and laser particle size distribution analysis showed that only a single spinel phase and a normal distribution pattern with the average size(D50) of 0.886μm could be observed.Due to the suitable partical size distribution,the Li4Ti5O12 powders showed a promising electrochemical performance.At the discharge current densities of 0.1C(16.5 mAh/g) and 5C,the discharge capacities reached 165 mAh/g and 107 mAh/g,respectively.Even at 10C,it still reached 54 mAh/g.作者联系地址：南开大学新能源材料化学研究所;天津巴莫科技股份有限公司;Author's Address: 1.Institute of New Energy Material Chemistry,Nankai University,Tianjin 300071,China;2.Tianjin B&M Science Technology Joint-Stock Co LTD,Tianjin 300384,Chin
