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L-异亮氨酸型配体交换固定相对DL-氨基酸的拆分研究
Authors
王俊德
王秋泉
黄晓佳
黄本立
Publication date
30 March 2005
Publisher
Abstract
用自制的新型L 异亮氨酸配体交换固定相在配体交换模式下对 11种DL 氨基酸进行了拆分研究,详细考察了流动相中铜离子浓度、甲醇含量、流速及温度对拆分效果的影响,并探讨了可能的拆分机理。研究结果表明:流动相中高浓度的铜离子不利于DL 氨基酸的拆分;增加流动相中甲醇的含量,降低流动相流速以及提高色谱柱温度均可改善拆分效果
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Last time updated on 16/06/2016