The sorption of Pd(II) on thiocarbamoylated propylpolysiloxane reaches the maximum value at pH=2.5, the highest degree of recovery of Au(III), Pt(IV) is observed in the pH=3-4 range with the combined presence of metal ions in the solution. The separation of Au(III) from platinum ions can be at pH=6.Благодарим Морозову Марию Витальевну за помощь в получении результатов на атомно-эмиссионном спектрометре