Conducting polyaniline nanotubes were synthesized by the oxidative polymerization of aniline with ammonium peroxydisulfate in water, in the presence of colloidal TiO2 nanoparticles of an average diameter ~5 nm. Polyaniline-TiO2 nanocomposite has been characterized by the electrical conductivity measurements, thermogravimetric analysis, FTIR spectroscopy, scanning and transmission electron microscopies. The electrical conductivity of synthesized nanocomposite was 1.1 × 10–3 S cm–1, slightly higher than that of pure polyaniline prepared under the same conditions. Polyaniline nanotubes have an outer diameter of 45–230 nm nm, an inner diameter of 15–130 nm, and a length extending from 0.5 to 2.0 μm.Physical chemistry 2008 : 9th international conference on fundamental and applied aspects of physical chemistry; Belgrade (Serbia); 24-28 September 200