Fatigue crack growth and fracture mechanics analysis of a working roll surface layer material is presented in this paper. The research is done on a hot strip mill working roll where High Chromium Steel is used for roll’s shell material. To obtain corresponding parameters, a rectangular single edge notched bend specimens – SENB, according to standard BS 7448, were used. The fatigue crack growth analysis was done on a resonant testing machine with use of special crack gauges, while for fracture mechanics parameters the electro–mechanical testing machine was used

I. Samardžić

M. Drobne

S. Glodež

T. Vuherer

English

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481METALURGIJA 53 (2014) 4, 481-484M. DROBNE, T. VUHERER, I. SAMARDŽIĆ, S GLODEŽFATIGUE CRACK GROWTH AND FRACTURE MECHANICS ANALYSIS OF A WORKING ROLL SURFACE LAYER MATERIALReceived – Primljeno: 2013-11-05Accepted – Prihvaćeno: 2014-04-30Original scientific paper – Izvorni znanstveni radISSN 0543-5846METABK 53(4) 481-484 (2014)UDC – UDK 620.178:539.375:621.771:669.15=111M. Drobne, Valji, production of rolls and castings d.o.o., Slovenia, T. Vuherer, University of Maribor, Faculty of Mechanical Engineering, Slovenia, I. Samardžić, University of Osijek, Mechanical Engineering Faculty, Slavonski Brod, Croatia, S. Glodež University of Maribor, Fac-ulty of Mechanical Engineering, Slovenia Fatigue crack growth and fracture mechanics analysis of a working roll surface layer material is presented in this paper. The research is done on a hot strip mill working roll where High Chromium Steel is used for roll’s shell mate-rial. To obtain corresponding parameters, a rectangular single edge notched bend specimens – SENB, according to standard BS 7448, were used. The fatigue crack growth analysis was done on a resonant testing machine with use of special crack gauges, while for fracture mechanics parameters the electro–mechanical testing machine was used. Key words: fracture mechanics, fatigue crack growth, rolling, high chromium steelINTRODUCTIONRolling is a metal forming process where metal is drawn into the rolling gap by using a pair of working rolls. Attaining the required plastic deformation of rolled metal is the main goal of a rolling process. In or-der to achieve this condition, working rolls must be manufactured and thermally treated in such a way that they will operate a certain service life under given load-ing condition [1, 2]. A variety of working rolls accord-ing to the dimensions, design and material properties could be chosen for different types of rolling stands. Working rolls which operate at the beginning of a roll-ing process in a hot strip mill, at reversible roughing 4 – high stands, are double layered. The 4 – high stand is composed of two working and two back up rolls. A carbide based cast steel material High Chromium Steel is used for hard and wear resistant working layer cast by using special centrifugal casting machine, while for the core a classic gravity casting procedure as a combina-tion of perlitic – feritic nodular graphite cast iron is used to assure the required toughness of roll’s core.SPECIFICS OF ROLLS LOADINGDue to operating conditions in 4 – high stands, rolls are thermo-mechanically loaded. When studying ther-mo-mechanical loads of rolls during one revolution, two types of stress and strain field could be considered in the contact. Stresses in the area between working and back up roll could describe the Hertzian contact theory between two elastic circle bodies and in the area be-tween working roll and rolled metal, which are wide-spread through the larger contact field. Thermal load-ings on working rolls result in rapid heat transfer from rolled metal to working roll in the time when contact between them is established. After the contact is estab-lished, surface temperature of the working roll falls quickly, because of water cooling. Schröder [3] investi-gated the temperature distribution during one revolution of the working roll. He showed that temperature chang-es from 600 °C to around 100 °C. Similar Belzunce et al. [4] concluded that with the rapid change of tempera-ture during rolling process, small fire cracks could ap-pear on working roll surface. In connection with me-chanical loadings especially at the contact between working and back up roll the appearance of fire cracks could lead to roll’s surface failure and breakage.Different types of failures could be noticed on work-ing rolls during their exploitation. A comprehensive in-vestigation among them is published in [5]. Due to high contact stresses between working and back up roll pres-sure cracks could appear near or on the working roll surface. In the next phase a fatigue fracture band propa-gates in the surface. Such fractures are called “Cat’s Tongue Spalls”, see Figure 1.All working roll failures have different kinds of ori-gins related either to roll manufacture or specific rolling conditions in the mill. Podgornik et al. [6] investigated different machining parameters and the influence of heat treatment on residual stress field and wear of dou-ble layer cast rolls. Their conclusions show that with Figure 1  A Cat’s Tongue Spall visible on working roll surface layer482  METALURGIJA 53 (2014) 4, 481-484M. DROBNE et al.: FATIGUE CRACK GROWTH AND FRACTURE MECHANICS ANALYSIS OF A WORKING ROLL...incorrect production phase a high tensile residual stress-es could be observed on working rolls surface layer. Simunovic et al. [7] exposed that with inappropriate surface roughness the possibility of surface cracks ap-pearance increases. In connection with conditions in rolling stands, tensile residual stresses and surface cracks could be fatal regarding the structural integrity of working rolls.EXPERIMENTAL TESTINGTheoretical backgroundTo understand the structural integrity of working roll, parameters of the fracture mechanics such as KIc – plane strain fracture toughness of the material, should be known and moreover, fatigue crack growth accord-ance with the number of working cycles should be ob-tained. In many structural components subjected to cy-clic loadings, critical growth often occurs due to fatigue until critical crack size is reached causing fracture [8]. Three regions could be observed when plotting the typ-ical fatigue crack growth curve, see Figure 2.Region 1 indicates the threshold value ∆Kth, below which there is no crack growth. In this region, micro-structure, mean stress and environment mainly control the crack growth. A linear relationship between fatigue crack growth rate log da/dN and applied stress intensity factor range log ∆K also known as Paris law [8] repre-sented in equation (1) could be observed in region 2 and corresponds to stable macroscopic crack growth. ( )mda C KdN= ⋅ ∆    (1)In region 3 the fatigue crack growth rates are very high as they approach instability. This region is prima-rily controlled by KIc.Experimental procedureDetermination of fracture mechanics parameters and fatigue crack growth curve was done at room tempera-ture which is related to the condition on the contact field between working and back up roll. All specimens SENB according to standard BS 7448 [9] were cut out of the working roll shell, by using abrasive water blast technol-ogy, and the wire erosion procedure was used for creating a notch. Therefore it is assumed that specimens have similar characteristics as the working roll. The width of the specimen W = 16 mm and its thickness B = 8 mm. Before experimental testing, chemical composition of HCS was determined by using an emission spectrom-eter Spectrolab, see Table 1, while mechanical material properties are presented in Table 2. Figure 3 shows a microstructure of HCS specimen etched with Vilella at 1000 x magnification before and after special heat treat-ment by using the Olympus DP 12 camera in the Olym-pus BX 51 M light microscope.Heat treatment of working rolls is composed of vari-ous quenching and tempering processes. From Figure 3 it is evident that with heat treatment, beside eutectic car-bides M7C3 segregated along grain boundaries, also sec-ondary M23C6 chromium carbides participate in the ma-trix. In combination with other carbides, chromium car-Figure 2 Typical fatigue crack growth curve with three regionsTable 1  Chemical composition of HCS determined with emission spectrometerElement C Si Mn P S Cr Ni Mo Cu V Fe% 1,75 0,68 0,74 0,027 0,037 11,55 1,94 1,13 0,14 0,25 restFigure 3 Microstructure of High Chromium Steel – HCS; a) before heat treatment, b) after heat treatment483METALURGIJA 53 (2014) 4, 481-484M. DROBNE et al.: FATIGUE CRACK GROWTH AND FRACTURE MECHANICS ANALYSIS OF A WORKING ROLL...bides contribute to the appropriate hardness, tensile/com-pression strength and wear resistance of the material. Fracture mechanics testing was performed at room temperature, on the electro–mechanical testing machine SCHENK TREBEL RM 100. Crack mouth opening dis-placement was registered by the special extensometer KLIP – GAGE DD1, the measuring accuracy of which is ± 0,001 mm. After testing, KIc was determined accord-ing to standard plane strain conditions described in [9]. The device for a crack increment registration FRAC-TOMAT was used for determination of fatigue crack growth curve. A special foil gauge RMF A – 5 was ap-plied on a specimen to register the change in electrical resistance.Table 2  Mechanical material properties at room temperatureTensile Strength Rm  / MPaCompressive Strength σc / MPaE / MPa ν930 2345 213 400 0,288RESULTSA fatigue crack length needed for determination KIc factor is presented in Figure 4. Surfaces of the speci-mens show that a brittle fracture is presented. In Figure 4b and Figure 4c some unusual curves of fatigue crack growth through the specimen thickness could be ob-served. This probably happened because HCS is a car-bide based material and when crack hits carbide, it could change the direction of propagation. Values of KIc for each specimen represented in Figure 4 are specified in Table 3. Table 3 KIc values for each specimen1 2 3 4KIc / MPa √–m 34,36 24,96 26,71 27,24The Fatigue crack growth curve for HCS is present-ed in Figure 5.Material parameters ∆Kth and KIc could be observed in Figure 5. In the region where stable crack growth is detected factors C and m, needed for Paris law equation, Figure 4 Fatigue crack length; a) Specimen 1, b) Specimen 2, c) Specimen 3, d) Specimen 4Figure 5 log da/dN – log ∆K dependency diagram for HCS484  METALURGIJA 53 (2014) 4, 481-484M. DROBNE et al.: FATIGUE CRACK GROWTH AND FRACTURE MECHANICS ANALYSIS OF A WORKING ROLL...could be determined. Values of coefficients and ∆Kth are given in Table 4. Table 4 Parameters C, m and ∆Kth∆Kth (MPa √–m) C  /( )m cycleMPa m    m4,84 8,0538 10-14 4,7398A small difference between ∆Kth and KIc could be observed, which reflects in low service life of working rolls with crack presence.CONCLUSIONFracture mechanics analysis and fatigue crack growth of a working roll surface layer material High Chromium Steel is presented in this article. All experi-mental investigation was performed as it is described in standard BS 7448 [9]. Before experimental testing a microstructure of HCS before and after heat treatment is presented.Results of the fracture mechanics analysis shows that when a crack is presented, a small load is needed for rupture and brittle fracture, which is proven with fracture surfaces presented in Figure 4 and with low values of KIc. After fracture mechanics analysis, the fa-tigue crack growth was determined. Results of the in-vestigation are presented in log da/dN – log ∆K dia-gram, Figure 5. ∆Kth coefficient could be observed from the diagram. There is a small difference between ∆Kth and KIc which reflects in low service life of roll with crack presence.Results presented in this study will serve as a basis for more comprehensive investigation related to roll’s microstructure influence on crack propagation.AcknowledgementOperation is part financed by the European Union, European Social Fund.REFERENCES[1] Lenard, G. F. Primer on Flat Rolling – A monograph for those who need to understand the basics of the flat rolling process. Elsevier, London, 2007.[2] ASM HANDBOOK Volume 14 Forming and Forging. ASM International, Novelty, Ohio 1996.[3] Schröder, K.H. Frequently Asked Questions about Hot Strip Mill Work Roll Surface. WMSP, 2004, New Orleans[4] Belzunce, F. J.; Ziadi, A.; Rodriguez, C.; Structural integri-ty of hot strip mill rolling rolls. Engineering Failure Analy-sis 11 (2004), pp. 789-797.[5] CAEF Roll Failure Manual; The European Foundry Asso-ciation, Roll Section; 1st Edition 2012.[6] Podgornik, B.; Milanović, S.; Vižintin, J. Effect of diffe-rent production phases on residual stress field in double-layer cast rolls. Journal of Materials Processing Technolo-gy, 210, 2010, pp. 1083-1088.[7] Simunovic, G.;Simunovic, K.; Saric, T.; Modelling and si-mulation of surface roughness in face milling; Internatio-nal Journal of Simulation Modelling 12 (2013), pp 141-153.[8] Glodež, S.; Flašker, J. Dimenzioniranje na življenjsko dobo: znanstvena monografija. Univerza v Mariboru, Ma-ribor, 2006.[9] BS 7448 - 1 Fracture mechanics toughness tests BSI, Lon-don, 1997.Note:  The responsible person for English is Urša Gavez, Štore, Slovenia

Fatigue crack growth and fracture mechanics analysis of a working roll surface layer material

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