Abstract

A paramount aspect in the development of a model for a monitoring system is the so-called parameter stability. This is inversely related to the uncertainty, i.e., the variance in the parameters estimates. Noise affects the performance of the monitoring system, reducing its fault detection capability. Low parameters uncertainty is desired to ensure a reduced amount of noise in the model. Nonetheless, there is no sound study on the parameter stability in batch multivariate statistical process control (BMSPC). The aim of this paper is to investigate the parameter stability associated to the most used synchronization and principal component analysis-based BMSPC methods. The synchronization methods included in this study are the following: indicator variable, dynamic time warping, relaxed greedy time warping, and time linear expanding/compressing-based. In addition, different arrangements of the three-way batch data into two-way matrices are considered, namely single-model, K-models, and hierarchicalmodel approaches. Results are discussed in connection with previous conclusions in the first two papers of the series.This research work was partially supported by the Spanish Ministry of Economy and Competitiveness under the project DPI2011-28112-C04-02. Authors also acknowledge the anonymous reviewers for their comments to improve the article.González Martínez, JM.; Camacho Páez, J.; Ferrer, A. (2014). Bilinear modeling of batch processes. Part III: Parameter Stability. Journal of Chemometrics. 28(1):10-27. https://doi.org/10.1002/cem.2562S1027281Process analysis and abnormal situation detection: from theory to practice. (2002). IEEE Control Systems, 22(5), 10-25. doi:10.1109/mcs.2002.1035214Statistical monitoring of multistage, multiphase batch processes. (2002). 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