Abstract The Objective of the present paper is to investigate the effect of electroless coating parameters, such as Sensitization time (A), Activation time (B) and Metallization time (C), on the coating morphology of the basalt short fiber and the optimization of the coating process parameters based on L 27 Taguchi orthogonal design. Coated and non-coated basalt short fiber, typically used with 7075 Aluminium alloy as reinforcement, is studied. The effect of coating the short basalt fiber with copper has proved beneficial to interfacial bonding (wettability) between the reinforcement and the matrix. The interface between the matrix and the reinforcement plays a crucial role in determining the properties of metal matrix composites (MMCs). An L 27 array was used to accommodate the three levels of factors as well as their interaction effects. From the Taguchi methodology, the optimal combinations for coating parameters were found to be A 1 B 3 C 3 (i.e., 5 min. sensitization time, 15 min. activation time and 3 min. for metallization time). In addition, the interaction between pH value and the coating time and that between the coating time and the temperature, influence the coating parameters significantly. Furthermore, a statistical analysis of variance reveals that the metallization time has the highest influence followed by the activation time and the sensitization time. Finally, confirmation tests were carried out to verify the experimental results, Scanning Electron Microscopic (SEM) & Energy Dispersive Spectroscope (EDS) studies were carried out on basalt fiber
