Fourier-transform infrared analysis and interpretation for bituminous binders

InfraRed spectrometry is a powerful technique to characterise bituminous binders. The methodology is not fully harmonised and may lead to vari-ability. The RILEM-272-PIM-TG1, evaluated seven complex bituminous, for which eleven laboratories performed FTIR. While, the spectra showed sim-ilar trends, further analysis was needed to improve comparison. A specific approach was applied on two binders, unmodified and polymer modified bitumen, and two ageing conditioning. Combining a Gaussian distributionand derivative analysis confirmed a good alignments of laboratory results. A two-step model was developed improving further interpretation. It con-sists of a baseline adjustment with eight points and normalisation over the maximum aliphatic peak. Furthermore, a specific fingerprint model was determined with the main absorption peaks defined by their location and shape. Only the intensity varies from laboratory to laboratory and binders. This general approach can be used as a platform to characterise aging or binder complexityGreen Open Access added to TU Delft Institutional Repository 'You share, we take care!' - Taverne project https://www.openaccess.nl/en/you-share-we-take-care Otherwise as indicated in the copyright section: the publisher is the copyright holder of this work and the author uses the Dutch legislation to make this work public.Pavement Engineerin

Complex bituminous binders, are current test methods suitable for?

The asphalt industry is constantly working to enhance the performances of asphalt materials, introducing innovative and more sustainable solutions. In this context, the incorporation of materials, such as additives, polymers, is more and more used to improve the properties of neat bitumen. This leads to even more complex bituminous binders, raising the question, are the current specifications and test methods appropriate for complex materials? To deal with this, the RILEM Technical Committee 272-PIM ‘Phase and Interphase behaviour of innovative bi-tuminous Materials’ with its Task Group TG1 is looking at the efficiency of vari-ous test methods for complex binders with an extensive inter-laboratory program with 17 laboratories. It includes seven different binders, two neat bitumen, two polymer modified bitumen and three binders with liquid additives, emphasising on compositional and physical changes at different conditions. The focus is low temperature; while a complementary experimental program encompasses as well as testing at intermediate and high temperatures. The outcomes of the work will provide indications on how robust the current binder characterisation techniques are and establish technical recommendations for future test methods specially de-signed for complex binders. Some first results are presented hereby.Accepted Author ManuscriptPavement Engineerin

Towards an enhanced fatigue evaluation of bituminous mortars

The fatigue resistance, as a performance indicator, is of paramount importance for the selection and benchmarking of bituminous materials. The bituminous mortar can be considered as the medium that connects and envelopes the coarse aggregate skeleton, and hence will significantly influence the fatigue resistance at bulk-scale. Therefore this study presents the steps and challenges of a new testing framework to evaluate the fatigue resistance of bituminous mortars. To do so, first, a new test geometry is introduced, which will ensure cohesive failure in a predefined area. The integrity of this sample geometry is assessed theoretically through finite element simulations and by computer tomography scans. Secondly, specimens of the new geometry are evaluated experimentally using a dynamic shear rheometer, where time-sweep tests are performed on two control mortar types under various test conditions. The control mortar types are fabricated using two commercial bituminous binders, one modified and one neat binder, to evaluate the effect of binder type. The test results are comprehensively analysed using fundamental dissipated energy-based concepts but also empirical and phenomenological failure criteria, providing insights into the failure evolution. For the tested mortar types, the analysis shows good convergence with the considered fatigue models. Finally, using dissipated energy concepts led to the most consisted fatigue model, which is independent of binder type and test conditions.Green Open Access added to TU Delft Institutional Repository ‘You share, we take care!’ – Taverne project https://www.openaccess.nl/en/you-share-we-take-care Otherwise as indicated in the copyright section: the publisher is the copyright holder of this work and the author uses the Dutch legislation to make this work public.Pavement Engineerin