169 research outputs found
Konjac Bio-Molecules Assisted, Rod-Spherical shaped Lead Nano Powder Synthesized by Electrolytic Process and Its Characterization Studies
Synthesis and structural characterization of Pb nanoparticles by electrolysis
using a bioactive compound - konjac aqueous extract is the main aim of this
study. This method is a unique, novel, low cost and double-step procedure with
good reproducibility and has not been used for nanoparticles preparation so
far. Konjac extract has been added to prevent the oxidation of Pb
nanoparticles. Also the synthesized nanoparticles have been dried in open air
to observe their stability. Various types of characterization tools like XRD,
SEM, Particle Size Analyzer, TEM-EDS, DSC, AAS and FT-IR have been utilized to
study characters of the end product. Anti-bacterial Studies has also been done.
After completion of synthesis process that we have made an attempt to change
the shape of the synthesized nanoparticles by the influence of sunbeams and to
find the effects of the sunlight on nanomaterials.Comment: 37 Pages, 20 Figures, 19 Tables, 20 Equations and 64 References.
arXiv admin note: text overlap with arXiv:1111.026
An Insight Analysis of Nano sized powder of Jackfruit Seed
The preparation of biodegradable nanomaterials by blending starch
nanocrystals with various polymer matrices are the most active research. This
work reports aspect related to nano-sized particles of jackfruit seed. This
approach is simple, faster, eco-friendly, cost effective and suitable for large
scale production. X-Ray Diffraction studies analyze particles size, morphology,
type of starch and degree of crystallinity. The particle size is found to be
12nm, specific surface area is 625 m2g-1, contains A-type starch and 32% degree
of crystallinity. A morphology index (MI) is developed from FWHM of XRD data to
understand interrelationship of particle size and specific surface area. MI
range is from 0.50 to 0.74. It is correlated with the particle size and
specific surface area. It is observed that MI has direct relationship with
particle size and an inverse relationship with specific surface area.Comment: 12 Pages, 5 Figures, 5 Table
Chemical Synthesis of Nano-Sized particles of Lead Oxide and their Characterization Studies
The quantum dots of semiconductor display novel and interesting phenomena
that have not been in the bulk material. The color tunability is one of the
most attractive characteristics in II-VI semiconductor nanoparticles such as
CdS, ZnS, CdSe, ZnSe and PbO. In this work, the semiconductor lead oxide
nanoparticles are prepared by chemical method. The average particle size,
specific surface area, crystallinity index are estimated from XRD analysis. The
structural, functional groups and optical characters are analyzed with using of
SEM, FTIR and UV- Visible techniques. The optical band gap value has also been
determined.Comment: 8 pages, 5 figures, 2 table
Cumulative effects of insecticides on generalist predators and parasitoid population in cocoa ecosystem
Please see the pdf file here: http://indsocplantationcrops.in/journal.ph
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