Nanoindentation characterization on local plastic response of Ti-6Al-4V under high-load spherical indentation

After high-load spherical indentation treatment, the variations of hardness on the plastic zone of Ti-6Al-4V were investigated via nanoindentation method. The hardness within the center of plastic zone was measured by nanoindenter, and the magnitude decreased gradually along the depth, which were caused by the different extent of plastic deformation under the residual imprint. The microstructure of indentation were observed using scanning electron microscope (SEM) before and after surface etching, and the results showed that the microhardness revealed the average hardness of α and β phases of Ti-6Al-4V. The maximum hardness reached 6.438 GPa in the depth of 132 μm. In addition, the two and three dimensional contour profiles of residual imprint introduced by high-load spherical indentation were measured by the white-light interferometer and the shape of residual imprint was obtained. All results were discussed in detail

Microstructure evolution and mechanical property response of TC11 titanium alloy under electroshock treatment

© 2020 The Authors This work investigated the effects of electroshock treatment (EST) on the microstructure variation and mechanical properties of TC11 alloy. The average hardness of the specimens decreased from 358 HV to 328 HV after EST of 0.04 s, then increased to 396 HV after EST of 0.06 s. After EST, the yield strength of specimen declined from 959 MPa to 797 MPa after EST of 0.04 s, and then increased to 1265 MPa after EST of 0.06 s, but the fracture strain decreased continuously. The variation in mechanical properties was closely related to the phase transition from the secondary α (αs) to β phase, and the precipitation of refined needlelike α martensite (αM). The diffusion of atoms accompanied by broaden αs/β boundary from 11.2 nm to 27.6 nm due to the phase transformation after EST by 0.04 s and the dislocation pileup at the boundary to form defects, which resulted the decrease in strength. While increasing the EST time to 0.06 s, the width of αM/β boundary decreased to 5.91 nm. All results indicated that the EST is an effective method for optimizing the microstructure and mechanical properties of titanium alloys in a short time

Novel approach of electroshock treatment for defect repair in near-β titanium alloy manufactured via directed energy deposition

© 2021, The Minerals, Metals & Materials Society and ASM International. A subsecond and novel approach of electroshock treatment (EST) is used in this study to repair defects in directed-energy-deposited Ti-5Al-5Mo-5V-3Cr-1Zr near-β titanium alloy. After EST, the porosity of the specimen decreased significantly from 0.81 to 0.1 pct. Large cracks observed at the bottom of the above mentioned near-β titanium alloy became intermittent small cracks and the number of voids decreased. The defects in the top and middle regions of the specimens are repaired. The potential defect repair is attributable to energy concentration, which promoted the coalescence of defect tips, and thermal stresses, which compressed the defects inward and closed them

Effects of shot peening on microstructure evolution and mechanical properties of surface nanocrystal layer on titanium matrix composite

Shot peening (SP) was employed to modify the surface microstructure and mechanical properties of (TiB+TiC)/Ti-6Al-4V titanium matrix composite (TMC). And the microstructure evolution and mechanical properties were characterized and analyzed in detail. Transmission electron microscopy (TEM) results illustrated that the surface nanograins were introduced by the effect of SP and the hindering of reinforcements to the matrix deformation. The nanograins were formed near the reinforcement/matrix interface because the matrix was squeezed by both the shots and the reinforcements. Moreover, with increasing the volume fraction of reinforcements, the smaller nanograins were introduced near the interfaces due to the severe deformation between the matrix and reinforcements, which were caused by the decrease in average distance between two reinforcements. Under the same intensity of SP, the deformation of TiC was more severe than that of TiB, and more dislocations were introduced around TiC. The results were influenced by both the different shapes and distribution of reinforcements, and the impact direction of shots. After SP, the compressive residual stress (CRS) and the hardness in the peened surface layer were improved, which was due to the surface deformation, nanograins and high dislocation density in the nanocrystal layer

Evaluation of microstructure variation of TC11 alloy after electroshocking treatment

Electro-shocking treatment (EST) has been investigated as a pathway to optimise the microstructure and mechanical properties of titanium alloys. The thermal conditions introduced by EST resulted in a phase transformation from α to β. The fraction of β phase decreased from 25.27% to 19.47% after EST for 0.02 s, which was possibly caused by the recrystallization of α phase. The application of EST for 0.04 s resulted in an increase in volume fraction of the β phase to 26.95%. The energy introduced by EST resulted in changes to the direction and intensity of texture within the microstructure with the texture intensity of the α phase increasing from 4.94 to 8.52, and that of β both increased from 3.35 to 9.88 after 0.04 s EST. © 2020 The Authors

Finite Element Dynamic Analysis on Residual Stress Distribution of Titanium Alloy and Titanium Matrix Composite after Shot Peening Treatment

The residual stress distribution introduced by shot peening (SP) in the deformed surface layer of Ti-6Al-4V and (TiB+TiC)/Ti-6Al-4V were simulated and studied via the three-dimensional (3D) finite element dynamic analysis and the experimental validation. The program of ANSYS/LS-DYNA was utilized, and the 3D homogeneous and inhomogeneous models were set up. The homogeneous model was established for simulating SP process on Ti-6Al-4V. The influence of three important parameters, the shot balls’ size, shot velocity and coverage rate on residual stress distribution were investigated. Numerical simulation results showed that these parameters contributed different effects on SP treatment. Using a simplified method, an inhomogeneous model for simulating SP process on (TiB+TiC)/Ti-6Al-4V was set up. The max tensile and compressive residual stress (CRS) was +1155 and −1511 MPa, respectively. Based on this stress distribution, the beneficial effect of reinforcements was indicated during deformation, retarding the damage to the matrix and keeping the adverse tensile stresses in the reinforcements. In order to verify the results of simulation, the residual stress distribution along depth was measured by X-ray diffraction (XRD) method. The residual stress distribution by experiments was agreed with the simulated results, which verified the availability of 3D finite element dynamic analysis

Electroshock treatment dependent microstructural evolution and mechanical properties of near-β titanium alloy manufactured by directed energy deposition

Effects of electroshock treatment (EST) on the microstructural evolution and mechanical properties of near-β titanium alloy (Ti-55531) formed by directed energy deposition (DED) was studied in this work. With the increase in EST time, the average hardness of specimen decreased from 426 HV to 316 HV, and the fracture strain increased significantly, which was attributed to the uniform dispersion of α phase along grain boundaries and inside the β grains. After EST, the texture intensity decreased in terms of the orientation distribution function (ODF), which was ascribed to the redistribution of α phase. Moreover, more atomic vacancies and lattice distortion were formed near the α/β interfaces, which were verified by transmission electron microscopy (TEM) observation and ascribed to the migration of atoms near the interface under EST. External loadings facilitated the dislocation motion and lattice distortions near the interfaces, which resulted in the reduction in hardness and the improvement in ductility. The above results indicated that EST can quickly alter the microstructure and mechanical properties of DED titanium alloys as a simple and energy-saving method

Grain boundary and texture evolution of TiB/Ti–2Al–6Sn titanium matrix composite under electroshocking treatment

This work used electroshocking treatment (EST) plus external loading to regulate the microstructure of titanium matrix composites (TMCs). The external loading was 0.3 MPa. After EST plus external loading with 0.3 MPa, the was reduced to 2.53 m in size. The percentage of high angle grain boundaries (HAGBs) in increased first and then decreased. The percent of HAGBs in TiB decreased, mainly due to the introduction of abundant dislocations in the TiB/matrix interface after EST. After EST, the maximum texture strength of TiB decreased from 13.09 to 12.97, and that of decreased from 3.11 to 1.58. After EST under external loading with 0.3 MPa, the maximum texture strength of TiB decreased to 8.10. The orientation of TiB experienced significant variation. TEM results showed that TiB and formed a distorted interface after EST under external loading with 0.3 MPa. The interplanar spacing of TiB and was varied. All results show that the texture of TMCs can be relieved by EST plus external loading with 0.3 MPa. It is mainly attributed to the thermal and athermal effects and the imposed external loads with EST. EST plus external loading provides a new method for manipulating the microstructure of TMCs