Effect of surface conditioning methods on the bond strength of luting cement to ceramics

Objectives. This study evaluated the effect of three different surface conditioning methods on the bond strength of a Bis-GMA based luting cement to six commercial dental ceramics. Methods. Six disc shaped ceramic specimens (glass ceramics, glass infiltrated alumina, glass infiltrated zirconium dioxide reinforced alumina) were used for each test group yielding a total number of 216 specimens. The specimens in each group were randomly assigned to one of the each following treatment conditions: (1) hydrofluoric acid etching, (2) airborne particle abrasion, (3) tribochemical silica coating. The resin composite luting cement was bonded to the conditioned and silanized ceramics using polyethylene molds. All specimens were tested at dry and thermocycled (6.000, 5-55degreesC, 30 s) conditions. The shear bond strength of luting cement to ceramics was measured in a universal testing machine (2 mm/min). Results. In dry conditions, acid etched glass ceramics exhibited significantly higher results (26.4-29.4 MPa) than those of glass infiltrated alumina ceramics (5.3-18.1 MPa) or zirconium dioxide (8.1 MPa) (ANOVA, P <0.001). Silica coating with silanization increased the bond strength significantly for high-alumina ceramics (8.5-21.8 MPa) and glass infiltrated zirconium dioxide ceramic (17.4 MPa) compared to that of airborne particle abrasion (ANOVA, P <0.001). Thermocycling decreased the bond strengths significantly after all of the conditioning methods tested. Significance. Bond strengths of the luting cement tested on the dental ceramics following surface conditioning methods varied in accordance with the ceramic types. Hydrofluoric acid gel was effective mostly on the ceramics having glassy matrix in their structures. Roughening the ceramic surfaces with air particle abrasion provided higher bond strengths for high-alumina ceramics and the values increased more significantly after silica coating/silanization. 2003 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved

An overview of development and status of fiber-reinforced composites as dental and medical biomaterials

Fibr-reinforced composites (FRC) have been used successfully for decades in many fields of science and engineering applications. Benefits of FRCs relate to physical properties of FRCs and versatile production methods, which can be utilized. Conventional hand lamination of prefabricated FRC prepregs is utilized still most commonly in fabrication of dental FRC devices but CAD-CAM systems are to be come for use in certain production steps of dental constructions and medical FRC implants. Although metals, ceramics and particulate filler resin composites have successfully been used as dental and medical biomaterials for decades, devices made out of these materials do not meet all clinical requirements. Only little attention has been paid to FRCs as dental materials and majority of the research in dental field has been focusing on particulate filler resin composites and in medical biomaterial research to biodegradable polymers. This is paradoxical because FRCs can potentially resolve many of the problems related to traditional isotropic dental and medical materials. This overview reviews the rationale and status of using biostable glass FRC in applications from restorative and prosthetic dentistry to cranial surgery. The overview highlights also the critical material based factors and clinical requirement for the succesfull use of FRCs in dental reconstructions

Resin-Bonded Fiber-Reinforced Composite for Direct Replacement of Missing Anterior Teeth: A Clinical Report

Missing anterior teeth is of serious concern in the social life of a patient in most of societies. While conventional fixed partial dentures and implant-supported restorations may often be the treatment of choice, fiber-reinforced composite (FRC) resins offer a conservative, fast, and cost-effective alternative for single and multiple teeth replacement. This paper presents two cases where FRC technology was successfully used to restore anterior edentulous areas in terms of esthetic values and functionality

Resin adjustment of three-dimensional printed thermoset occlusal splints: Bonding properties - Short communication

Objectives: To evaluate the interfacial adhesion of an autopolymerizing acrylic resin to 3D printed thermoset occlusal splints compared to thermoplastic occlusal splints.Materials and methods: Cylinders made of an autopolymerizing acrylic resin were adhered to 3D printed thermoset and also to thermoplastic plates. A different surface treatment and three storage conditions were used: dry, 7 days water-storage and 14 days water-storage. Bond strength test (so-called shear-bond strength test) was afterward performed.Results: ANOVA (R2 = 0.764) revealed significant differences in bond strength according to material (p Conclusions: The bond strength of autopolymerizing acrylic resin to 3D printed thermoset plates is higher when compared to thermoplastic plates. Bonding between acrylic resin and 3D printed splints was high enough for clinical applications.conclusion</div

Impact of Fast High-Intensity versus Conventional Light-Curing Protocol on Selected Properties of Dental Composites

To study the influence of fast high-intensity (3-s) and conventional (20-s) light curing protocols on certain physical properties including light-transmission and surface wear of two nano-hybrid composite resins (Tetric PowerFill and Essentia U) specifically designed for both curing protocols. According to ISO standards, the following properties were investigated: flexural properties, fracture toughness and water sorption/solubility. FTIR-spectrometry was used to calculate the double bond conversion (DC%). A wear test using a chewing simulator was performed with 15,000 chewing cycles. A tensilometer was used to measure the shrinkage stress. Light transmission through various thicknesses (1, 2, 3 and 4 mm) of composite resins was quantified. The Vickers indenter was utilized for evaluating surface microhardness (VH) at the top and the bottom sides. Scanning electron microscopy was utilized to investigate the microstructure of each composite resin. The light curing protocol did not show a significant (p > 0.05) effect on the mechanical properties of tested composite resins and differences were material-dependent. Shrinkage stress, DC% and VH of both composite resins significantly increased with the conventional 20 s light curing protocol (p </p

The Effect of Exposed Glass Fibers and Particles of Bioactive Glass on the Surface Wettability of Composite Implants

Measurement of the wettability of a material is a predictive index of cytocompatibility. This study was designed to evaluate the effect of exposed E-glass fibers and bioactive glass (BAG) particles on the surface wettability behavior of composite implants. Two different groups were investigated: (a) fiber reinforced composites (FRCs) with different fiber orientations and (b) polymer composites with different wt. % of BAG particles. Photopolymerized and heat postpolymerized composite substrates were made for both groups. The surface wettability, topography, and roughness were analyzed. Equilibrium contact angles were measured using the sessile drop method. Three liquids were used as a probe for surface free energy (SFE) calculations. SFE values were calculated from contact angles obtained on smooth surfaces. The surface with transverse distribution of fibers showed higher (P < 0.001) polar (γP) and total SFE (γTOT) components (16.9 and 51.04 mJ/m2, resp.) than the surface with in-plane distribution of fibers (13.77 and 48.27 mJ/m2, resp.). The increase in BAG particle wt. % increased the polar (γP) value, while the dispersive (γD) value decreased. Postpolymerization by heat treatment improved the SFE components on all the surfaces investigated (P < 0.001). Composites containing E-glass fibers and BAG particles are hydrophilic materials that show good wettability characteristics