30 research outputs found
Depth-Sensing Indentation on REBa2Cu3O(7-\delta) Single Crystals obtained from Xenotime Mineral
A natural mixture of heavy rare earths oxides extracted from xenotime mineral
have been used to prepare large single crystals of high-temperature
REBa2Cu3O(7-\delta) superconductor grown using the CuO-BaO self-flux method.
Its mechanical properties along the ab-plane were characterized using
instrumented indentation. Hardness and elastic modulus were obtained by the
Oliver and Pharr method and corresponds to 7.4 \pm 0.2 GPa and in range 135-175
GPa at small depths, respectively. Increasing the load promotes the nucleation
of lateral cracks that causes a decrease in hardness and the measured elastic
modulus by instrumented indentation at higher loads. The indentation fracture
toughness was estimated by measuring the radial crack length from cube-corner
indentations at various loads and was 0.8 \pm 0.2 MPa.m1/2. The observed slip
systems of REBa2Cu3O(7-\delta) single crystals were [100](001) and [010](001),
the same as for YBa2Cu3O(7-\delta) single crystals. The initial stages of
deformation and fracture in the indentation process were investigated. The
hardness and elastic modulus were not strongly modified by the crystallographic
orientation in the ab-plane. This was interpreted in terms of the resolved
shear stresses in the active slip systems. Evidence of cracking along the {100}
and {110} planes on the ab-plane was observed. As a conclusion, the mechanical
properties of REBa2Cu3O(7-\delta) single crystals prepared from xenotime are
equivalent to those of YBa2Cu3O(7-\delta) single crystals produced by
conventional rare earths oxides.Comment: The paper will appear in Volume 42 (2012) of the Brazilian Journal of
Physic