The Microstructural Characterization of Semi-Solid Slurries

Due to recent interest in semi-solid metal (SSM) processing, there is a need for fundamental knowledge on the formation and solidification of primary particles. The primary particle size, distribution, morphology, and percentage are the main concerns because particle quantity and size affect not only the mechanical properties of as-cast SSM parts but also the flow characteristics of SSM slurries during die filling. Microstructural characterization is a basic tool for measuring the critical parameters that influence the resulting properties. This article describes the tools and techniques available for structural analysis of SSM slurries. It also attempts to elucidate the ambiguities and interpretations of special structural features.Shahrooz Nafisi and Reza Ghomashch

In situ Three-Dimensional microstructural investigation of solidification of an Al-Cu alloy by ultra-fast X-Ray microtomography

This article presents the first results of a new experimental technique developed to investigate the evolution of the morphology of the solid and liquid phases during the solidification of a metallic alloy. It consists of ultrafast X-ray microtomography observations of a solidifying aluminum-copper alloy carried out at ESRF. These experiments allow investigating in-situ the formation of the casting microstructure and of the evolution of the morphology of the solid and the liquid phases. It allows also the in-situ determination of the solidification path, of the variation of the copper content in both the liquid and solid phases, and of some other characteristic parameters of the microstructure. Provided that some forthcoming technical improvements on the experimental setup are performed, more quantitative results can be obtained as well as better image quality and resolution