This paper described the determination of amygdalin in sweet and bitter almond kernel in Erbil City using GC-FID technique. The effect of wavelength, selecting the best solvent as a mobile phase, flow rate, injection volume, pH, and temperature had been studied, in which the flow rate 10.0 ml min-1 at the concentration range (20-600) μg ml-1 with correlation coefficient and relative error (0.9990, 1.501%)respectively