Analysis of thermal degradation behavior for some hydraulic oils, using FTIR-TGA coupling

The transitions between the vibrational energetic states of atoms represent the infrared absorption spectra, which is a band spectrum over which the transitions between energetic rotational states overlap. One of the most important uses of infrared absorption spectrometry is the identification in quantitative terms of the structure of compounds from a substance, the analytes being either solid, liquid or vaporous. The FTIR-TGA Coupling is a technique that permanently controls the mass loss in a sample, as a function of temperature and time, as well as the identification and recording of various compounds occurring during the combustion process. Research on hydraulic oils has consisted of their analysis using the FTIR-TGA coupling in order to identify flammable substances that can generate explosive events

Assessing the heavy metal pollution level in Jiu Valley by bio-monitoring inferior plants – moss

The analysis of the samples collected from residential areas and the proximity of the industrial areas of Jiu Valley was carried out by means of induced coupled plasma optical emission spectrometry (ICP-OES) after acid processing and mineralization of the samples. The pollution level has increased once with the industrial development and acceleration of urbanization processes in the human society. Of the pollutant-generating substances, heavy metals are of particular importance. The purpose of this paper is to highlight level of pollution by heavy metals using moss (inferior plants) in order to determine the degree of bioaccumulation. From the pollution point of view, zinc, cadmium and lead are of particular relevance, but the effects of other heavy metals have also been studied. The pollution effects last for a long time in waste dumps, areas polluted with heavy metals from fuel combustion processes, fossil fuels a.s.o. The analysis of the samples collected from residential areas and the proximity of the industrial areas of Jiu Valley was carried out by means of induced coupled plasma optical emission spectrometry (ICP-OES) after acid processing and mineralization of the samples

Analysis of thermal degradation behavior for some hydraulic oils, using FTIR-TGA coupling

The transitions between the vibrational energetic states of atoms represent the infrared absorption spectra, which is a band spectrum over which the transitions between energetic rotational states overlap. One of the most important uses of infrared absorption spectrometry is the identification in quantitative terms of the structure of compounds from a substance, the analytes being either solid, liquid or vaporous. The FTIR-TGA Coupling is a technique that permanently controls the mass loss in a sample, as a function of temperature and time, as well as the identification and recording of various compounds occurring during the combustion process. Research on hydraulic oils has consisted of their analysis using the FTIR-TGA coupling in order to identify flammable substances that can generate explosive events

Assessing the heavy metal pollution level in Jiu Valley by bio-monitoring inferior plants – moss

The analysis of the samples collected from residential areas and the proximity of the industrial areas of Jiu Valley was carried out by means of induced coupled plasma optical emission spectrometry (ICP-OES) after acid processing and mineralization of the samples. The pollution level has increased once with the industrial development and acceleration of urbanization processes in the human society. Of the pollutant-generating substances, heavy metals are of particular importance. The purpose of this paper is to highlight level of pollution by heavy metals using moss (inferior plants) in order to determine the degree of bioaccumulation. From the pollution point of view, zinc, cadmium and lead are of particular relevance, but the effects of other heavy metals have also been studied. The pollution effects last for a long time in waste dumps, areas polluted with heavy metals from fuel combustion processes, fossil fuels a.s.o. The analysis of the samples collected from residential areas and the proximity of the industrial areas of Jiu Valley was carried out by means of induced coupled plasma optical emission spectrometry (ICP-OES) after acid processing and mineralization of the samples

Determination of the chemical composition of the residual powder in order to identify the source of release

Particles in suspension come mainly from pollutant emissions generated by industry, traffic, home heating, etc. Due to these particles, various diseases can occur, such as lung cancer, asthma, cardiovascular diseases. An important problem is represented by the particles with an aerodynamic diameter of less than 10 micrometers, which pass through the nose and throat and enter the alveoli of the lungs causing inflammation and intoxication. This paper aimed to establish the chemical composition of residual powders in a production hall from the automotive industry, to identify the source of release. For this, the infrared spectrometry (FTIR) method, the inductively coupled plasma optical emission spectrometry (ICP-OES) method, and the x-ray spectrometry (XRF) method were used. Two samples of dust from different locations of the production hall were analyzed, as well as a substance used in the process, to determine whether the dust came from its use. A series of safety data sheets for substances used in the technological process was also analyzed. The results obtained from the qualitative and quantitative determinations were evaluated considering the chemical composition of all substances involved, leading to the identification of the residual dust release source

Heavy metal pollution from dust deposits in urban and industrial areas in the Jiul Valley

The aim of this paper was to determine the concentration of heavy metals in dust samples by the method of analysis by inductively coupled plasma optical emission spectrometry (ICP-OES) and to assess the degree of pollution of the studied areas. The dust samples studied and subjected to analytical analyzes were collected from the vicinity of industrial areas and urban areas of localities in the Jiu Valley, a monoindustrial area. The main heavy metals determined were: Cu, Zn, Pb, Ni, Cr, Co etc. Dust particles depending on their origin can be inorganic or organic. The samples were collected from the urban areas and from the vicinity of the industrial areas