Comparison of dynamic fatigue behavior between SiC whisker-reinforced composite and monolithic silicon nitrides

The dynamic fatigue behavior of 30 vol percent silicon nitride whisker-reinforced composite and monolithic silicon nitrides were determined as a function of temperature from 1100 to 1300 C in ambient air. The fatigue susceptibility parameter, n, decreased from 88.1 to 20.1 for the composite material, and from 50.8 to 40.4 for the monolithic, with increasing temperature from 1100 to 1300 C. A transition in the dynamic fatigue curve occurred for the composite material at a low stressing rate of 2 MPa/min at 1300 C, resulting in a very low value of n equals 5.8. Fractographic analysis showed that glassy phases in the slow crack growth region were more pronounced in the composite compared to the monolithic material, implying that SiC whisker addition promotes the formation of glass rich phases at the grain boundaries, thereby enhancing fatigue. These results indicate that SiC whisker addition to Si3 N4 matrix substantially deteriorates fatigue resistance inherent to the matrix base material for this selected material system

Issues of advanced ceramic matrix composites in aeroengine applications

Ceramic matrix composites (CMCs) are enabling propulsion material systems for hot-section components of advanced aeroengines for improvement in power and fuel efficiency due to their higher temperature capability and much lighter weight as compared to current metallic counterparts. However, there are still persistent issues regarding transition and maturation of CMCs to engine applications, attributed to their susceptibility to environmental degradation in harsh engine operations. These environment-associated issues include foreign object damage (FOD), erosion, sand dust (‘CMAS’), and themomechanical and thermochemical loading/reactions, all leading to material degradation with its degree depending on the condition or austerity of engine operations. These issues need to be explored and taken into account for design of related material systems and components as well. Some of these issues including FOD, erosion, sand dust, and thermomechanical aspects will be presented and discussed as to how they have effects in advanced, gas-turbine grade SiC/SiC CMCs that are currently considered as engine component materials

Mechanical behavior and failure phenomenon of an in situ-toughened silicon nitride

The Weibull modulus, fracture toughness and crack growth resistance of an in-situ toughened, silicon nitride material used to manufacture a turbine combustor were determined from room temperature to 1371 C. The material exhibited an elongated grain structure that resulted in improved fracture toughness, nonlinear crack growth resistance, and good elevated temperature strength. However, low temperature strength was limited by grains of excessive length (30 to 100 microns). These excessively long grains were surrounded by regions rich in sintering additives

Dynamics of tilt-based browsing on mobile devices

A tilt-controlled photo browsing method for small mobile devices is presented. The implementation uses continuous inputs from an accelerometer, and a multimodal (visual, audio and vibrotactile) display coupled with the states of this model. The model is based on a simple physical model, with its characteristics shaped to enhance usability. We show how the dynamics of the physical model can be shaped to make the handling qualities of the mobile device fit the browsing task. We implemented the proposed algorithm on Samsung MITs PDA with tri-axis accelerometer and a vibrotactile motor. The experiment used seven novice users browsing from 100 photos. We compare a tilt-based interaction method with a button-based browser and an iPod wheel. We discuss the usability performance and contrast this with subjective experience from the users. The iPod wheel has significantly poorer performance than button pushing or tilt interaction, despite its commercial popularity

Cyclic Fatigue of Brittle Materials with an Indentation-Induced Flaw System

The ratio of static to cyclic fatigue life, or 'h ratio', was obtained numerically for an indentation flaw system subjected to sinusoidal loading conditions. Emphasis was placed on developing a simple, quick lifetime prediction tool. The solution for the h ratio was compared with experimental static and cyclic fatigue data obtained from as-indented 96 wt.% alumina specimens tested in room-temperature distilled water

Reconciling the shadow of a subduction signature with rift geochemistry and tectonic environment in Eastern Marie Byrd Land, Antarctica

Basalt-trachyte volcanoes in the Marie Byrd Land (MBL) Cenozoic province lie along the Amundsen Sea coast on the north flank of the West Antarctic rift. Basalts here are characterized by OIB-like geochemistry, restricted ranges of 87Sr/86Sr (0.702535–0.703284) and 143Nd/144Nd (0.512839–0.513008) and a wide range of 206Pb/204Pb (19.357–20.934). Basalts at three MBL volcanoes display two anomalies compared with the above and with all other basalts in West Antarctica. They include 143Nd/144Nd (0.512778–0.512789) values at Mt. Takahe and Mt. Siple that are 2σ lower than other West Antarctic basalts, and Ba/Nb, Ba/La, and Ba/Th values at Mt. Murphy and Mt. Takahe that are 3–8 times higher than normal OIB. Isotope and trace element data do not support crustal and lithospheric mantle contamination, or the presence of residual mantle amphibole or phlogopite as explanations of these anomalies. The apparent coincidence of these anomalies with the site of a pre-Cenozoic convergence zone along the Gondwanaland margin suggests a subduction influence. Major episodes of subduction and granitic plutonism took place in MBL during the Devonian, Permian, and Late Cretaceous. Relicts in the source region, of components from these subducted slabs, provide a credible explanation for the uncoupling of Ba from other large ion lithophile elements (LILE), for its erratic distribution, and for the anomalously low 143Nd/144Nd at Mt. Takahe. The last episode of subduction ended ~ 85 Ma, and was followed by continental break-up, rifting and lithospheric attenuation that produced the West Antarctic rift as we know it today. Thus, the enigmatic geochemical signatures in these three volcanoes seem to have been preserved roughly 61–85 m.y. after subduction ended. New calculations of source melting depth and a new determination of lithospheric thickness suggest that the source of the anomalies resides in a fossil mélange diapir that rose from the Cretaceous subducting slab, became attached to the base of the lithosphere at 80–100 km depth, and remained there during the subsequent plate motion and source remobilization history of this region

Assessments of Fracture Toughness of Monolithic Ceramics-SEPB Versus SEVNB Methods

Fracture toughness of a total of 13 advanced monolithic ceramics including silicon nitrides, silicon carbide, aluminas, and glass ceramic was determined at ambient temperature by using both single edge precracked beam (SEPB) and single edge v-notched beam (SEVNB) methods. Relatively good agreement in fracture toughness between the two methods was observed for advanced ceramics with flat R-curves; whereas, poor agreement in fracture toughness was seen for materials with rising R-curves. The discrepancy in fracture toughness between the two methods was due to stable crack growth with crack closure forces acting in the wake region of cracks even in SEVNB test specimens. The effect of discrepancy in fracture toughness was analyzed in terms of microstructural feature (grain size and shape), toughening exponent in R-curve, and stable crack growth determined using back-face strain gaging

Apparatus for Hot Impact Testing of Material Specimens

An apparatus for positioning and holding material specimens is a major subsystem of a system for impact testing of the specimens at temperatures up to 1,500 C. This apparatus and the rest of the system are designed especially for hot impact testing of advanced ceramics, composites, and coating materials. The apparatus includes a retaining fixture on a rotating stage on a vertically movable cross support driven by a linear actuator. These components are located below a furnace wherein the hot impact tests are performed (see Figure 1). In preparation for a test, a specimen is mounted on the retaining fixture, then the cross support is moved upward to raise the specimen, through an opening in the bottom of the furnace, to the test position inside the furnace. On one side of the furnace there is another, relatively small opening on a direct line to the specimen. Once the specimen has become heated to the test temperature, the test is performed by using an instrumented external pressurized-gas-driven gun to shoot a projectile through the side opening at the specimen

Accelerated Testing Methodology Developed for Determining the Slow Crack Growth of Advanced Ceramics

Constant stress-rate ("dynamic fatigue") testing has been used for several decades to characterize the slow crack growth behavior of glass and structural ceramics at both ambient and elevated temperatures. The advantage of such testing over other methods lies in its simplicity: strengths are measured in a routine manner at four or more stress rates by applying a constant displacement or loading rate. The slow crack growth parameters required for component design can be estimated from a relationship between strength and stress rate. With the proper use of preloading in constant stress-rate testing, test time can be reduced appreciably. If a preload corresponding to 50 percent of the strength is applied to the specimen prior to testing, 50 percent of the test time can be saved as long as the applied preload does not change the strength. In fact, it has been a common, empirical practice in the strength testing of ceramics or optical fibers to apply some preloading (<40 percent). The purpose of this work at the NASA Lewis Research Center is to study the effect of preloading on measured strength in order to add a theoretical foundation to the empirical practice