Experimental characterisation of the local mechanical behaviour of cellulose fibres: an in‑situ micro‑profilometry approach

The accurate mechanical characterisation of fibres of micrometric length is a challenging task, especially in the case of organically-formed fibres that naturally exhibit considerable irregularities along the longitudinal fibre direction. The present paper proposes a novel experimental methodology for the evaluation of the local mechanical behaviour of organically-formed (aged and unaged) and regenerated cellulose fibres, which is based on in-situ micro-tensile testing combined with optical profilometry. In order to accurately determine the cross-sectional area profile of a cellulose fibre specimen, optical profilometry is performed both at the top and bottom surfaces of the fibre. The evolution of the local stress at specific fibre locations is next determined from the force value recorded during the tensile test and the local cross-sectional area. An accurate measurement of the corresponding local strain is obtained by using Global Digital Height Correlation (GDHC), thus resulting in multiple, local stress--strain curves per fibre, from which local tensile strengths, elastic moduli, and strains at fracture can be deduced. Since the variations in the geometrical and material properties within an individual fibre are comparable to those observed across fibres, the proposed methodology is able to attain statistically representative measurement data from just one, or a small number of fibre samples. This makes the experimental methodology very suitable for the mechanical analysis of fibres taken from valuable and historical objects, for which typically a limited number of samples is available. It is further demonstrated that the accuracy of the measurement data obtained by the present, local measuring technique may be significantly higher than for a common, global measuring technique since possible errors induced by fibre slip at the grip surfaces are avoided

A computational framework for the lifetime prediction of vertical-axis wind turbines:CFD simulations and high-cycle fatigue modeling

A novel computational framework is presented for the lifetime prediction of vertical-axis wind turbines (VAWTs). The framework uses high-fidelity computational fluid dynamics (CFD) simulations for the accurate determination of the aerodynamic loading on the wind turbine, and includes these loading characteristics in a detailed 3D finite element method (FEM) model to predict fatigue cracking in the structure with a fatigue interface damage model. The fatigue interface damage model allows to simulate high-cycle fatigue cracking processes in the wind turbine in an accurate and robust fashion at manageable computational cost. The FEM analyses show that the blade-strut connection is the most critical structural part for the fatigue life of the VAWT, particularly when it is carried out as an adhesive connection (instead of a welded connection). The sensitivity of the fatigue response of the VAWT to specific static and fatigue modeling parameters and to the presence of a structural flaw is analyzed. Depending on the flaw size and flaw location, the fatigue life of the VAWT can decrease by 25%. Additionally, the decrease of the fatigue resistance of the VAWT appears to be mainly characterized by the monotonic reduction of the tensile strength of the adhesive blade-strut connection, rather than by the reduction of its mode I toughness, such that fatigue cracking develops in a brittle fashion under a relatively small crack opening. It is emphasized that the present computational framework is generic; it can also be applied for analyzing the fatigue performance of other rotating machinery subjected to fluid–structure interaction, such as horizontal-axis wind turbines, steam turbine generators and multistage pumps and compressors

Automated image segmentation of 3D printed fibrous composite micro-structures using a neural network

A new, automated image segmentation method is presented that effectively identifies the micro-structural objects (fibre, air void, matrix) of 3D printed fibre-reinforced materials using a deep convolutional neural network. The method creates training data from a physical specimen composed of a single, straight fibre embedded in a cementitious matrix with air voids. The specific micro-structure of this strain-hardening cementitious composite (SHCC) is obtained from X-ray micro-computed tomography scanning, after which the 3D ground truth mask of the sample is constructed by connecting each voxel of a scanned image to the corresponding micro-structural object. The neural network is trained to identify fibres oriented in arbitrary directions through the application of a data augmentation procedure, which eliminates the time-consuming task of a human expert to manually annotate these data. The predictive capability of the methodology is demonstrated via the analysis of a practical SHCC developed for 3D concrete printing, showing that the automated segmentation method is well capable of adequately identifying complex micro-structures with arbitrarily distributed and oriented fibres. Although the focus of the current study is on SHCC materials, the proposed methodology can also be applied to other fibre-reinforced materials, such as fibre-reinforced plastics. The micro-structures identified by the image segmentation method may serve as input for dedicated finite element models that allow for computing their mechanical behaviour as a function of the micro-structural composition

Effect of accelerated curing and layer deformations on structural failure during extrusion-based 3D printing

Recent experimental research by Reiter et al. (Cem. Concr. Res., 132:106047, 2020) indicates that the buildability of fresh concrete used in extrusion-based 3D printing processes can be significantly enhanced by chemically accelerating the curing process. In the present contribution the effect of accelerated curing on failure by plastic collapse and elastic buckling during 3D concrete printing is explored by incorporating a power-law curing function in the parametric 3D printing model developed by Suiker (Int. J. Mech Sci, 137:145–170, 2018). A structural yield criterion is derived for the case of accelerated curing, and the main advantages on the resistance against plastic collapse are demonstrated through a comparison of the predicted failure characteristics to those for linear curing and exponentially-decaying curing. Subsequently, the elastic buckling behaviour under accelerated curing is derived for a free wall configuration, and the competition between elastic buckling and plastic collapse of the free wall structure is assessed via the construction of failure mechanism maps. In addition, a modelling recipe is proposed for consistently accounting for the vertical deformations of layers in the prediction of structural failure during 3D concrete printing. The modelling of this effect may further increase the accuracy of the prediction of the number of layers at structural failure. For failure under plastic collapse, results are computed for linear curing, exponentially-decaying curing and accelerated curing. The model outcome for linear curing is used for a comparison with results from 3D concrete printing experiments recently presented in the literature, showing an excellent agreement. It is further demonstrated that the effect of vertical wall deformations on the prediction of failure by elastic buckling typically is minor, so that for this failure mechanism this contribution may be left out of consideration. All design graphs presented in this communication are generic, in a sense that they are not restricted to concrete, but can be applied for other printing materials as well

Numerical modelling of climate-induced fracture and deformation in wood: Application to historical museum objects

Damage in oak wood museum objects under indoor climate variations (relative humidity, temperature) is studied using a thermo-hygro-mechanical model. The model incorporates the effects of moisture sorption hysteresis and discrete cracking, and is implemented within a finite element framework using a staggered update procedure. Sorption experiments were performed in order to calibrate the moisture sorption hysteresis model. The basic features of the coupled formulation are stepwisely demonstrated by solving the response of a basic oak wood specimen under a sequence of thermo-hygro-mechanical loading conditions of increasing complexity. These simulations show that the deformation and fracture generated by thermal variations representative of indoor museum conditions are minor compared to the contributions caused by relative humidity variations. Subsequently, the hygro-mechanical response of an oak wood cabinet door panel is analysed under a drop in relative humidity from 60% to 20%, and the results are compared to those obtained by experiments. The numerical and experimental results are in good agreement, and indicate that at the connection between the cleated end and the vertical boards the restrained hygric shrinkage is maximal, which stimulates local crack development. The susceptibility to fracture only becomes activated after the oak wood has reached a certain age, as the effect of aging induces a decrease of the oak wood tensile strength perpendicular to the grain direction with time. Further, when the initial moisture content lies on the desorption boundary curve, the amount of fracture generated is larger compared to when it lies on the adsorption boundary curve. Also, fracture only nucleates after a specific drop in relative humidity, whereby the crack growth under a continuous decrease in relative humidity initially develops relatively fast, but at a certain stage decreases substantially and becomes (almost) zero when reaching a fully developed failure crack. The location and orientation of this failure crack are in accordance with in situ observations on historical oak wood cabinets

Crack channelling mechanisms in brittle coating systems under moisture or temperature gradients

Crack channelling is predicted in a brittle coating-substrate system that is subjected to a moisture or temperature gradient in the thickness direction. Competing failure scenarios are identified, and are distinguished by the degree to which the coating-substrate interface delaminates, and whether this delamination is finite or unlimited in nature. Failure mechanism maps are constructed, and illustrate the sensitivity of the active crack channelling mechanism and associated channelling stress to the ratio of coating toughness to interfacial toughness, to the mismatch in elastic modulus and to the mismatch in coefficient of hygral or thermal expansion. The effect of the ratio of coating to substrate thickness upon the failure mechanism and channelling stress is also explored. Closed-form expressions for the steady-state delamination stress are derived, and are used to determine the transition value of moisture state that leads to unlimited delamination. Although the results are applicable to coating-substrate systems in a wide range of applications, the study focusses on the prediction of cracking in historical paintings due to indoor climate fluctuations, with the objective of helping museums developing strategies for the preservation of art objects. For this specific application, crack channelling with delamination needs to be avoided under all circumstances, as it may induce flaking of paint material. In historical paintings, the substrate thickness is typically more than ten times larger than the thickness of the paint layer; for such a system, the failure maps constructed from the numerical simulations indicate that paint delamination is absent if the delamination toughness is larger than approximately half of the mode I toughness of the paint layer. Further, the transition between crack channelling with and without delamination appears to be relatively insensitive to the mismatch in the elastic modulus of the substrate and paint layer. The failure maps developed in this work may provide a useful tool for museum conservators to identify the allowable indoor humidity and temperature fluctuations for which crack channelling with delamination is prevented in historical paintings

Influence of morphology on the effective hygro-elastic properties of softwood (spruce) and hardwood (balsa)

Wood materials are characterized by complex hierarchical material structures spanning across various length scales. The present work aims at establishing a relation between the hygro-elastic properties at the mesoscopic cellular level and the effective material response at the macroscopic level, both for softwood (spruce) and hardwood (balsa). The particular aim is to explore the influence on the effective hygro-elastic properties under variations in the meso-scale morphology. The multi-scale framework applied for this purpose uses the method of asymptotic homogenization, which allows to accurately and efficiently obtain the effective response of heterogeneous materials characterized by complex meso-structural geometries. The meso-structural model considered for softwood is based on a periodic, two-dimensional statistically representative volume element that is generated by a spatial repetition of tracheid cells. The tracheid cells are modeled as hexagonal elements characterized by a certain geometrical irregularity. The hardwood meso-structure consists of a region composed of hexagonal cellular fibers with large vessels embedded, which is connected to a ray region that is constructed of ray cells. The hardwood fibers are modeled as hexagonal cellular elements, similar to softwood tracheids. The rays are represented by quadrilateral cells oriented along the radial direction, whereby different arrangements are considered, i.e., the ray cells are either regularly stacked or organized as a staggered configuration. The interface between the fiber and ray regions may also be characterized by a regular or a staggered arrangement. The meso-structural models for softwood and hardwood are discretized by means of plane-strain, finite element models, which describe the hygro-elastic response of the wood material in the radial–tangential plane. For softwood, the sensitivity of the effective elastic and hygro-expansive properties is explored as a function of the geometrical irregularity of the tracheids. For hardwood, the effective properties are studied under a variation of the ray cell arrangement, the type of interface between ray and fiber regions, and the vessel volume fraction. The modeling results agree well with results obtained from other numerical homogenization studies and show to be in reasonable agreement with experimental data taken from the literature