33 research outputs found

    Obtaining molybdenum-copper composite for effective thermal control in electronic systems

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    In the article, the molybdenum and copper powders, obtained by electric explosion of wires and plasma-dynamic method, respectively, were sintered by spark plasma sintering technology, in order to obtain bulk sample based on them. X-ray diffractometry and scanning electron microscopy were carried out to study the chemical composition and structure of the resulting ceramics. XRD analysis showed that the product consisted of the following main phases such as molybdenum of a cubic crystalline structure (space group Im3m, No. 229) and copper of cubic system (space group Fm-3m, No. 225). The results of scanning electron microscopy indicated that the sintered sample had heterogeneous structure with the presence of small pores. Nonetheless, the mechanical properties such as hardness (Vickers hardness of 292 HV) and thermal conductivity (140.53 W / m · °С) are good enough that allows considering the proposed synthesizing methods as well as sintering technology as promising for creating the Cu-Mo ceramics with high-mechanical properties

    Creating a varistor based on zinc oxide (ZNO) powder, obtained by plasma dynamic method

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    Zinc Oxide (ZnO) is a perspective material. This paper shows the results on synthesis of hexagonal zinc oxide and it's application

    Creating a varistor based on zinc oxide (ZNO) powder, obtained by plasma dynamic method

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    Zinc Oxide (ZnO) is a perspective material. This paper shows the results on synthesis of hexagonal zinc oxide and it's application

    The Possibility of Obtaining Materials by Plasma Dynamic Synthesis in the Ti-O System

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    The possibility of obtaining a dispersed material by the method of plasma dynamic synthesis in the Ti-O system is shown. The plasma dynamic synthesis is based on the operation of a pulsed high-current coaxial magnetoplasma accelerator with titanium electrodes. The obtained product was investigated by X-ray diffraction method and transmission electron microscopy. The results showed the presence of two main titanium oxide (IV) crystalline modifications: anatase with tetragonal syngony and rutile also with tetragonal syngony. Moreover, the dominant modification is anatase in synthesized material

    Modification of aluminum alloy surface properties by wave-long laser texturing

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    Change of the static contact angle (SCA) of 10 [mu]L distilled water droplet on laser textured aluminium alloy (AMG-6) substrates was studied. The texture was deposited by a laser system based on a fiber laser. An increase in the power of laser radiation is found to lead to a decrease in the SCA measured on the first day after texturing. Change of dispersion and polar surface energy components of textured substrates is determined. Under the influence of the environment, the surface properties of AMG-6 change with time. SCA increased and reached stable state on the twentieth day after texturing

    Plasma dynamic synthesis of iron oxides in the «frequency operation» mode of coaxial magnetoplasma accelerator

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    It is known that the epsilon phase of iron oxide e-Fe2O3 has the highest value of coercive force among all known simple metal oxides (~24 kOe) and is characterized by ferromagnetic resonance in the frequency range from 100 to 200 GHz. The noted features determine the possibility of its wide application. However, there is the problem of synthesis and stabilization this crystal structure at room temperature. In this paper, we consider the possibility to obtain e-Fe2O3 by the plasma dynamic method when the system is operating in the frequency (multi-pulse) regime. The influence of the number power supply impulses on the phase composition of the synthesized products was studied using X-ray diffractometry

    Plasma dynamic synthesis of ultradispersed copper oxides

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    Copper oxide is necessary material for production of superconductors. The issue of obtaining high purity and nanosides CuO is actual. This article shows the results on the obtaining of nanodispersed copper oxide by plasma dynamic method in system based on coaxial magneto plasma accelerator with copper electrodes. Such analyses of ultradispersed synthesized products as X-Ray diffractometry, IR-spectroscopy and thermal analysis were carried out. According to XRD such phases as copper Cu, copper oxide (I) Cu[2]O, copper oxide (II) CuO, and copper hydroxide hydrate Cu(OH)[2]xH[2]O were identified in the product. It was found that with the gradual heating of the initial product up to 800°С the phase content changed dramatically in terms of enhancing copper oxide phase (up to 97%)

    The plasma dynamic synthesis of aluminum nitride in system with gaseous and solid precursors

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    Aluminum nitride is widely-used material for semiconductor devices and ceramics production. Despite the large number of known ways to obtain AlN powder, the problem of synthesizing high-purity and nanosized product is still urgent. This paper shows results on plasma dynamic synthesis of aluminum nitride using system based coaxial magneto plasma accelerator. The influence of using gaseous or solid precursors on such characteristics of the final product as phase content and particle size distribution was investigated. According to X-Ray diffractometry AlN phase content is increased in the case of use of solid nitrogen-containing precursor (melamine) in comparison with the use of gaseous nitrogen. The particle sizes distribution histograms are built in accordance with the data of bright-field TEM-images and shown in this paper. The most of particles are less than 100 nm in both experiment but there are some differences, depended on the precursor type, that are also described
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