2k Factorial Experiments on Factors that Influence the Recovery of Gold during the Upgrade of Ilesha-Itagunmodi Gold Ore through Froth Flotation

A low-grade gold ore from Ilesha-Itagunmodi, south western Nigeria was panned, dried and ball-milled before sieving into fractions. The morphological, mineralogical and chemical composition was studied by optical micro-scopy (Reflected and Transmission), X-ray diffraction (XRD) and Energy Dispersive X-ray fluorescence (XRF), respectively. The sieved fractions were subjected to chemical analysis (AAS). The +106 μm sieve had the highest concentration of the mineral and was then selected for the upgrade through froth flotation using standard rea-gents. In this paper a report on a 2k factorial experiment that provides an understanding of the impact of opera-tional variables on the quantity of gold mineral obtained from the ore during froth flotation is presented. Analy-sis results showed that Ilesha-Itagunmodi gold ore is non-refractory with fine grain particles, amenable to froth flotation and contained about 20 other associated minerals, gold had a concentration of about 0.0024%. A com-bination of P-Xanthate and amine glycol collectors at a pH of 9.2 only produced a considerable increase in gold yield. This translated to about 87.13% increase in recovery of gold from the ore. Analysis of variance (ANOVA) was carried out and the model equation obtained was subsequently optimised to obtain a model equation that could be used in predicting the recoverable quantity of gold, indicating that F11,1-values for Collector concentra-tion, Frother concentration, pH and Conditioning time were 156.86, 6.96, 43.81, and 56.77 respectively. A model with an F value of 88.41 was obtained which indicated that the model was significant. The model equation obtained was subsequently optimised to be able to predict the recoverable quantity of gold. A “Pred R-Squared” value of 0.9365 (93.65%) was also obtained and is in reasonable agreement with the “Adj R-Squared” value of 0.9534 (95.34%). It was established that Ilesha placer gold ore is amenable to froth flotation using standard reagents

Impact behavior of spark plasma sintered Ti–Al–Mo/TiN composites: a finite element analysis approach using Abaqus CAE

Abstract Background The utilization of Finite Element Analysis (FEA) has emerged as a crucial methodology in the field of structural and elasticity analysis, facilitating researchers in their understanding of material responses to diverse thermal or structural loads. This study investigates the utilization of FEA to simulate the Impact characteristics of titanium composites, with specific emphasis on the Charpy impact test. The research utilizes the Abaqus Explicit software, which is widely recognized for its explicit dynamic analysis functionalities, to simulate high-speed and short-duration events such as impacts. The primary objective of this study is to examine the impact behavior of Ti–7Al–1mo/TiN composites fabricated through the spark plasma sintering technique. The impact behavior is simulated using FEA, wherein the shear failure model is utilized to replicate fracture phenomena. This paper examines the methodology employed in the FEA approach, with a particular focus on various factors including boundary conditions, explicit dynamic analysis settings, and material properties. Results The outcomes and analyses involve the examination of the von Mises stress distribution, displacement magnitude, and energy behavior of the models that were tested. Reinforcement of Ti–Al–Mo ternary alloy with TiN led to a progressive increase in maximum von Mises stress, reaching a peak at 3 wt% TiN. Conversely, displacement magnitude decreased with increasing TiN content, with CP-Ti and the unreinforced alloy exhibiting the highest values. Absorbed energy also declined with higher TiN levels. While models containing 5 and 7 wt% TiN displayed limited plastic deformation before fracture, composites with ≤ 3 wt% TiN maintained acceptable ductility despite enhanced strength and stiffness. Conclusion The FEA methodology effectively simulates the Charpy impact characteristics of Ti–7Al–1Mo/TiN composites, thereby offering significant contributions to understanding their mechanical behaviors. These findings suggest that TiN reinforcement up to 3 wt% presents a promising strategy for improving the mechanical performance of Ti–Al–Mo alloys while minimizing the trade-off in toughness. This research emphasizes the inherent trade-off between toughness and strength/stiffness, suggesting the possibility of optimizing the composition of materials to suit particular applications. This study makes a valuable contribution to the expanding field of impact behavior research, demonstrating the potential of FEA, specifically utilizing Abaqus Explicit software, for enhancing material design and evaluation