Vertical hydraulic conductivity of a clayey-silt aquitard: accelerated fluid flow in a centrifuge permeameter compared with in situ conditions

This discussion paper is a preprint. It has been under review for the journal Hydrology and Earth System Sciences (HESS). The revised manuscript was not accepted.Evaluating the possibility of leakage through low permeability geological strata is critically important for sustainable water supplies, extraction of fuels from strata such as coal beds, and confinement of waste within the earth. Characterizing low or negligible flow rates and transport of solutes can require impractically long periods of field or laboratory testing, but is necessary for evaluations over regional areas and over multi-decadal timescales. The current work reports a custom designed centrifuge permeameter (CP) system, which can provide relatively rapid and reliable hydraulic conductivity (K) measurement compared to column permeameter tests at standard gravity (1g). Linear fluid velocity through a low K porous sample is linearly related to g-level during a CP flight unless consolidation or geochemical reactions occur. The CP module is designed to fit within a standard 2 m diameter, geotechnical centrifuge with a capacity for sample dimensions of 30 to 100 mm diameter and 30 to 200 mm in length. At maximum RPM the resultant centrifugal force is equivalent to 550g at base of sample or a total stress of ~2 MPa. K is calculated by measuring influent and effluent volumes. A custom designed mounting system allows minimal disturbance of drill core samples and a centrifugal force that represents realistic in situ stress conditions is applied. Formation fluids were used as influent to limit any shrink-swell phenomena which may alter the resultant K value. Vertical hydraulic conductivity (Kv) results from CP testing of core from the sites in the same clayey silt formation varied (10−7 to 10−9 m s−1, n = 14) but higher than 1g column permeameter tests of adjacent core using deionized water (10−9 to 10−11 m s−1, n = 7). Results at one site were similar to in situ Kv values (3 × 10−9 m s−1) from pore pressure responses within a 30 m clayey sequence in a homogenous area of the formation. Kv sensitivity to sample heterogeneity was observed, and anomalous flow via preferential pathways could be readily identified. Results demonstrate the utility of centrifuge testing for measuring minimum K values that can contribute to assessments of geological formations at large scale. The importance of using realistic stress conditions and influent geochemistry during hydraulic testing is also demonstrated.Australian Research CouncilNational Water Commissio

Accelerated gravity testing of aquitard core permeability and implications at formation and regional scale

Evaluating the possibility of leakage through low-permeability geological strata is critically important for sustainable water supplies, the extraction of fuels from coal and other strata, and the confinement of waste within the earth. The current work demonstrates that relatively rapid and realistic vertical hydraulic conductivity (Kv) measurements of aquitard cores using accelerated gravity can constrain and compliment larger-scale assessments of hydraulic connectivity. Steady-state fluid velocity through a low-K porous sample is linearly related to accelerated gravity (g level) in a centrifuge permeameter (CP) unless consolidation or geochemical reactions occur. A CP module was custom designed to fit a standard 2 m diameter geotechnical centrifuge (550 g maximum) with a capacity for sample dimensions up to 100 mm diameter and 200 mm length, and a total stress of  ∼  2 MPa at the base of the core. Formation fluids were used as influent to limit any shrink–swell phenomena, which may alter the permeability. Kv results from CP testing of minimally disturbed cores from three sites within a clayey-silt formation varied from 10−10 to 10−7  m s−1 (number of samples, n = 18). Additional tests were focussed on the Cattle Lane (CL) site, where Kv within the 99 % confidence interval (n = 9) was 1.1 × 10−9 to 2.0 × 10−9 m s−1. These Kv results were very similar to an independent in situ Kv method based on pore pressure propagation though the sequence. However, there was less certainty at two other core sites due to limited and variable Kv data. Blind standard 1 g column tests underestimated Kv compared to CP and in situ Kv data, possibly due to deionised water interactions with clay, and were more time-consuming than CP tests. Our Kv results were compared with the set-up of a flow model for the region, and considered in the context of heterogeneity and preferential flow paths at site and formation scale. Reasonable assessments of leakage and solute transport through aquitards over multi-decadal timescales can be achieved by accelerated core testing together with complimentary hydrogeological monitoring, analysis, and modelling

Developing methods to evaluate odour control products

An economical and practical alternative to the standard end-of-pipe odour control methods is the application of liquid odour control products. Currently, there are no established product-testing methods. The data that are available are often of questionable quality and may have limited relevance to waste management. Waste facilities receive differing streams of waste at varying loading volumes. Whilst in operation this exposes control products to a wide variety of environmental conditions, further increasing the difficulty of selecting an effective means of control. The current study initially identifies commercially available odour control products applicable for solid and liquid waste management operations. Bench-scale batch absorption tests have been carried out to investigate odorous gas abatement for a range of selected commercial products and water at a range of pH values. Hydrogen sulphide was the test odorous gas, as it is commonly associated with waste processes. Gas-phase volumetric mass-transfer coefficients (K(G)a) have been calculated to determine mass-transfer performance. The development of a pilot-scale spray tower is then presented as the testing apparatus for future work. This is an attempt to construct a repeatable testing method for evaluating abatement performance of odour control products, and control the problems encountered when applying odour control products to open sites. K(G)a values and data collected from tests in this study will be considered in future work as design parameters for the rig

A novel centrifuge permeameter to characterize flow through low permeability strata

A novel Centrifuge Permeameter (CP) system was designed to characterize and model seepage and reactive solute transport through low permeability materials and geological strata. A new CP module for the Broadbent G18 geotechnical centrifuge (2.0 m diameter), provides new capability for hydraulic conductivity (K) and transport testing of materials including drill cores, mine tailings and engineered barriers. By designing centrifuge models that maintain chemical equilibrium, reactive transport of solutes can be assessed within a reasonable experiment time at accelerated gravity. The K of minimally disturbed drill cores or porous materials having a diameter of 65-100 mm and a length of 20-200 mm can be measured using steady state flow, with a K detection limit currently within the order of 10-12 m/s. This paper presents K values as a function of depth below ground for drill core, and K as a function of effective porosity of reconstituted silica flour specimens. © 2010 Taylor & Francis Group, London

A novel centrifuge permeameter to characterize flow through low permeability strata

A novel Centrifuge Permeameter (CP) system was designed to characterize and model seepage and reactive solute transport through low permeability materials and geological strata. A new CP module for the Broadbent G18 geotechnical centrifuge (2.0 m diameter), provides new capability for hydraulic conductivity (K) and transport testing of materials including drill cores, mine tailings and engineered barriers. By designing centrifuge models that maintain chemical equilibrium, reactive transport of solutes can be assessed within a reasonable experiment time at accelerated gravity. The K of minimally disturbed drill cores or porous materials having a diameter of 65-100 mm and a length of 20-200 mm can be measured using steady state flow, with a K detection limit currently within the order of 10-12 m/s. This paper presents K values as a function of depth below ground for drill core, and K as a function of effective porosity of reconstituted silica flour specimens. © 2010 Taylor & Francis Group, London