Temperature dependence of the impurity-induced resonant state in Zn-doped Bi_2Sr_2CaCu_2O8+δ_{8+\delta} by Scanning Tunneling Spectroscopy

We report on the temperature dependence of the impurity-induced resonant state in Zn-doped Bi_2Sr_2CaCu_2O$_{8+\delta}$ by scanning tunneling spectroscopy at 30 mK < T < 52 K. It is known that a Zn impurity induces a sharp resonant peak in tunnel spectrum at an energy close to the Fermi level. We observed that the resonant peak survives up to 52 K. The peak broadens with increasing temperature, which is explained by the thermal effect. This result provides information to understand the origin of the resonant peak.Comment: 4 pages, 3 figures, to appear in Phys. Rev.

Single grain (LRE)-Ba-Cu-O superconductors fabricated by top seeded melt growth in air

We have recently reported a practical processing method for the fabrication in air of large, single grain (LRE)-Ba-Cu-O [where LRE Nd, Sm, Eu and Gd] bulk superconductors that exhibit high Tc and high Jc. The process is based initially on the development of a new type of generic seed crystal that can promote effectively the epitaxial nucleation of any (RE)-Ba-Cu-O system and, secondly, by suppressing the formation of (LRE)/Ba solid solution in a controlled manner within large LRE-Ba-Cu-O grains processed in air. In this paper we investigate the degree of homogeneity of large grain Sm-Ba-Cu-O superconductors fabricated by this novel process. The technique offers a significant degree of freedom in terms of processing parameters and reproducibility in the growth of oriented single grains in air and yields bulk samples with significantly improved superconducting and field-trapping properties compared to those processed by conventional top seeded melt growth (TSMG)

Effect of La Doping on Microstructure and Critical Current Density of MgB2

In the present study, La-doped MgB_2 superconductors with different doping level (Mg1-xLaxB2; x=0.00, 0.01, 0.03 & 0.05) have been synthesized by solid-state reaction route at ambient pressure. Effect of La doping have been investigated in relation to microstructural characteristics and superconducting properties, particularly intragrain critical current density (Jc). The microstructural characteristics of the as synthesized Mg(La)B2 compounds were studied employing transmission electron microscopic (TEM) technique. The TEM investigations reveal inclusion of LaB6 nanoparticles within the MgB2 grains which provide effective flux pinning centres. The evaluation of intragrain Jc through magnetic measurements on the fine powdered version of the as synthesized samples reveal that Jc of the samples change significantly with the doping level. The optimum result on Jc is obtained for Mg0.97La0.03B2 at 5K, the Jc reaches ~1.4x107A/cm2 in self field, ~2.1 x 106A/cm2 at 1T, ~2.5 x 105A/cm2 at 2.5T and ~1.8 x 104 A/cm2 at 4.5T. The highest value of intragrain Jc in Mg0.97La0.03B2 superconductor has been attributed to the inclusion of LaB6 nanoparticles which are capable of providing effective flux pinning centres

Local transport characteristics of break junction in Sr(2)RuO(4) microbridge

We have measured tunnel conductance of spin-triplet superconductor Sr(2)RuO(4) (SRO) break junction which was made by micro fabrication technique with a focused ion beam. This is a new type of tunnel junctions made of SRO, which is different from those made of SRO and other materials. Since the tunnel conductance is sensitive to the internal phase of superconductivity, it enables us to examine the chiral p-wave pairing state, which is the most probable candidate of SRO. The tunnel conductance spectrum of the junction showed a broad zero-bias conductance peak whose shape is different from that of high-T(c) cuprate superconductors. The shape of the spectrum is in quite good agreement with the calculated spectrum of a chiral p-wave/insulator/normal metal junction.ArticlePHYSICA C-SUPERCONDUCTIVITY AND ITS APPLICATIONS. 471(21-22):708-710 (2011)journal articl

Microstructure and superconducting properties of hot isostatically pressed MgB2

Bulk samples of MgB2 have been formed by hot isostatic pressing (HIPping) of commercial powder at 100MPa and 950=B0C. The resulting material is 100% dense with a sharp superconducting transition at 37.5K. Microstructural studies have indicated the presence of small amounts of second phases within the material, namely MgO and B rich compositions, probably MgB4. Magnetisation measurements performed at 20K have revealed values of Jc=1.3 x 106A/cm2 at zero field, and 9.3 x 105A/cm2 at 1T. Magneto optical (MO) studies have shown direct evidence for the superconducting homogeneity and strong intergranular current flow in the material.Comment: 3 pages, 6 figures, text updated, new references included and discussed. Submitted to Superconductor Science and Technolog

Anisotropic Superconducting Properties of MgB2 Single Crystals

In-plane electrical transport properties of MgB2 single crystals grown under high pressure of 4-6 GPa and temperature of 1400-1700oC in Mg-B-N system have been measured. For all specimens we found sharp superconducting transition around 38.1-38.3K with transition width within 0.2-0.3K. Estimated resistivity value at 40K is about 1 mkOhmcm and resistivity ratio R(273K)/R(40K) of about 4.9. Results of measurements in magnetic field up to 5.5T perpendicular to Mg and B planes and up to 9T in parallel orientation show temperature dependent anisotropy of the upper critical field with anisotropy ratio increasing from 2.2 close to Tc up to about 3 below 30K. Strong deviation of the angular dependence of Hc2 from anisotropic mass model has been also found.Comment: 10pages, including 5 figures,submitted to Physica C (in press

Superconducting thin films of MgB2 on (001)-Si by pulsed laser deposition

Superconducting thin films have been prepared on Si-substrates, using pulsed laser deposition from a target composed of a mixture of Mg and MgB2 powders. The films were deposited at room temperature and post-annealed at 600 degrees C. The zero resistance transition temperatures were 12 K, with an onset transition temperature of 27 K. Special care has been taken to avoid oxidation of Mg in the laser plasma and deposited film, by optimizing the background pressure of Ar gas in the deposition chamber. For this the optical emission in the visible range from the plasma has been used as indicator. Preventing Mg from oxidation was found to be essential to obtain superconducting films

Current percolation and anisotropy in polycrystalline MgB2_2

The influence of anisotropy on the transport current in MgB$_2$ polycrystalline bulk samples and wires is discussed. A model for the critical current density is proposed, which is based on anisotropic London theory, grain boundary pinning and percolation theory. The calculated currents agree convincingly with experimental data and the fit parameters, especially the anisotropy, obtained from percolation theory agree with experiment or theoretical predictions.Comment: 5 pages, accepted for publication in Physical Review Letters (http://prl.aps.org/

Evidence for high inter-granular current flow in single-phase polycrystalline MgB2 superconductor

The distribution of magnetic field in single-phase polycrystalline bulk MgB2 has been measured using a Magneto-Optical (MO) technique for an external magnetic field applied perpendicular to the sample surface. The MO studies indicate that an inter-granular current network is readily established in this material and the current is not limited by weak-linked grain boundaries. The grain boundaries are observed to resist preferential magnetic field penetration, with the inter-grain mechanism dominating the current flow in the sample at temperatures up to 30K. The results provide clear evidence that the intra-granular current flow is isotropic. A critical current density of ~10^4 Acm-2 was estimated at 30K in a field of 150mT from the MO measurements. These results provide further evidence of the considerable potential for MgB2 for engineering applications.Comment: 3 pages, 3 figure