346 research outputs found

    Electrical and Magnetic behaviour of PrFeAsO0.8F0.2 superconductor

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    The superconducting and ground state samples of PrFeAsO0.8F0.2 and PrFeAsO have been synthesised via easy and versatile single step solid state reaction route. X-ray & Reitveld refine parameters of the synthesised samples are in good agreement to the earlier reported value of the structure. The ground state of the pristine compound (PrFeAsO) exhibited a metallic like step in resistivity below 150K followed by another step at 12K. The former is associated with the spin density wave (SDW) like ordering of Fe spins and later to the anomalous magnetic ordering for Pr moments. Both the resistivity anomalies are absent in case of superconducting PrFeAsO0.8F0.2 sample. Detailed high field (up to 12Tesla) electrical and magnetization measurements are carried out for superconducting PrFeAsO0.8F0.2 sample. The PrFeAsO0.8F0.2 exhibited superconducting onset (Tconset) at around 47K with Tc({\rho} =0) at 38K. Though the Tconset remains nearly invariant, the Tc({\rho} =0) is decreased with applied field, and the same is around 23K under applied field of 12Tesla. The upper critical field (Hc2) is estimated from the Ginzburg Landau equation (GL) fitting, which is found to be ~ 182Tesla. Critical current density (Jc) being calculated from high field isothermal magnetization (MH) loops with the help of Beans critical state model, is found to be of the order of 103 A/cm2. Summarily, the superconductivity characterization of single step synthesised PrFeAsO0.8F0.2 superconductor is presented.Comment: 15 Pages Text + Fig

    A nod in the wrong direction : Does nonverbal feedback affect eyewitness confidence in interviews?

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    Eyewitnesses can be influenced by an interviewer's behaviour and report information with inflated confidence as a result. Previous research has shown that positive feedback administered verbally can affect the confidence attributed to testimony, but the effect of non-verbal influence in interviews has been given little attention. This study investigated whether positive or negative non-verbal feedback could affect the confidence witnesses attribute to their responses. Participants witnessed staged CCTV footage of a crime scene and answered 20 questions in a structured interview, during which they were given either positive feedback (a head nod), negative feedback (a head shake) or no feedback. Those presented with positive non-verbal feedback reported inflated confidence compared with those presented with negative non-verbal feedback regardless of accuracy, and this effect was most apparent when participants reported awareness of the feedback. These results provide further insight into the effects of interviewer behaviour in investigative interviewsPeer reviewedFinal Accepted Versio

    Structural, Magnetic and Magneto-caloric studies of Ni50Mn30Sn20Shape Memory Alloy

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    We have synthesized a nominal composition of Ni50Mn30Sn20 alloy using arc melting technique. Rietveld refinement confirms the austenite L21 structure in Fm-3m space group. Electrical resistivity has been found to clearly exhibiting two different phenomena viz. a magnetic transition from paramagnetic to ferromagnetic and a structural transition from austenite to martensitic phase. Thermo-magnetization measurements M(T) confirms ferromagnetic transition temperature TC at 222 K and martensitic transition starting at 127 K(MS). Magnetization measurement M(H) at 10 K confirms the ferromagnetic state. Frequency dependence of ac susceptibility \c{hi}' at low temperature suggests spin glass behavior in the system. The isothermal magnetic entropy change values have been found to be 1.14 J/Kg.K, 2.69 J/Kg.K and 3.9 J/Kg.K, with refrigeration capacities of 19.6 J/kg, 37.8 J/kg and 54.6 J/kg for the field change of 1, 2 and 3 Tesla respectively at 227 K.Comment: 16 pages text + Figs. Ni50Mn30Sn20 alloy: reasonable refrigeration capacity tunable to Room

    A COMPREHENSIVE REVIEW ON PHARMACEUTICAL AND NUTRITIONAL APPLICATIONS OF INULIN

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    Inulin is a versatile, water-soluble polysaccharide that is commonly available in nature. In the pharmaceutical industry, the non-digestible function of inulin has made it attractive. Inulin is granted with GRAS status by the FDA and more than 30,000 plants in nature store inulin as a carbohydrate. The chicory is the key plant source of inulin out of all sources. It can be used as the sugar or fat replacer in the processed foods to influence the desirable characteristics. Good biocompatibility, essential chemical properties, and a wide variety of bioactivities have rendered inulin an outstanding natural nutrient. Regulating blood sugar, antioxidant, anticancer is some of the biological activities of inulin. Inulin can also be a carrier for colon/tumor targeting, as only specific enzymes in the colon zhydrolyze the inulin. It allows the growth of micro-flora, the good bacteria in the gut. Inulin is considered as a prebiotic as it is fermented by bacteria that normalize the colon. This review offers an in-depth insight into its novel Pharmaceutical applications as well as sources, processing, physicochemical properties, and nutritional and physiological activities. The chemically modified inulin is gaining a specific interest in the pharmaceutical field with its outstanding properties which are discussed in this review
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