21 research outputs found

    BiFeO 3

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    The crystal and magnetic structure of BiFeO3BiFeO_3 have been studied with the use of high resolution neutron diffraction between 5 K and 300 K. The atomic coordinates in BiFeO3BiFeO_3 are almost unchanged between 5 K and 300 K

    BiFeO3BiFeO_3 Crystal Structure at Low Temperatures

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    The crystal and magnetic structure of BiFeO3BiFeO_3 have been studied with the use of high resolution neutron diffraction between 5 K and 300 K. The atomic coordinates in BiFeO3BiFeO_3 are almost unchanged between 5 K and 300 K

    Investigation of Crystal and Magnetic Structure of BiFeO3\text{}_{3} Using Neutron Diffraction

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    Polycrystalline material obtained from the ground single crystal of BiFeO3\text{}_{3} reported as not having the superstructure, shows the superstructure reflections in neutron diffraction pattern. The determined magnetic moment of antiferromagnetically ordered Fe3+\text{}^{3+} ions is μFe\text{}_{Fe} = (3.70±0.03)μB\text{}_{B} at 293 K

    Thermal Lattice Parameters Variation of CaCuxMn7xO12CaCu_xMn_{7-x}O_{12} Compounds with Trigonal Crystal Structure

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    We report the crystal structure evolution of CaCu0.2Mn6.8O12CaCu_{0.2}Mn_{6.8}O_{12} as a function of temperature between 10 K and 290 K. The analysis of the diffraction data is carried out with the Rietveld method applied to the average trigonal structure of CaCu0.2Mn6.8O12CaCu_{0.2}Mn_{6.8}O_{12}. The x = 0.2 member shows similar low temperature extrema for the unit cell parameter evolution as the previously reported x = 0.1 and x = 0 members of the CaCuxMn7xO12CaCu_xMn_{7-x}O_{12} system. All magnetic and crystallographic transition temperatures indicated by the unit cell parameter evolution obtained by powder X-ray diffraction methods systematically decrease with increasing Cu content, x

    Domain size effects in neutron and SR powder diffraction studies of some oxides

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    We discuss the properties of synchrotron radiation (SR) and neutron powder diffraction investigations of the crystal and magnetic structure of solids. Special emphasis is paid to the analysis of the full width at half maximum (FWHM) of the observed Bragg reflections and its relation with the size of the coherently ordered regions of the material. Two specific examples are discussed: a SR powder diffraction study of the crystal structure of the hexaferrite BaSn2Fe4O11 and a neutron powder diffraction study of the magnetic ordering of the magnetic moments of manganese ions in the distorted perovskite system CaMn7O12
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