15 research outputs found

    Study to Fabricate the Large Scale Buckypaper Based on Carbon Nanotubes

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    Carbon nanotubes (CNTs) have attracted great attention because of their unique structural, electrical, mechanical and thermal properties. Then CNTs have potential application as electrode for batteries and supercapacitors, especially binder-free electrodes. The major challenge is to fabricate the large scale electrode with the uniform thickness, electrical property. The large scale CNTs buckypaper can be fabricated via vacuum filtration technique. The characteristics of CNT dispersion and buckypaper depend on variety of factor such as sonication power, sonication time, dispersant…. In this study, we investigate the multiwall carbon nanotubes (MW CNTs) in Isopropanol (IPA) solvent with different sonication conditions, membrane filter size for paper with areal density of 3 mg/cm2 with different sizes such as 4, 10, 20 cm in diameter and large scale of 30x30 cm2. It is observed that the dispersion of CNTs are good and the thickness, conductivity are uniform over whole sample for above sizes. We also can get the highest conductivity of buckypaper was 3.9x103 S/m in 30 mins. It is found that the higher sonication power and higher sonication time are better for buckypaper

    Synthesis of Gold Nanobipyramids by Seed-mediated Method and Santibacterial Activities

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    Metallic nanoparticles as antibacterial agents have been studied for several years. The most used antibacterial nanoparticles are silver nanoparticles. The mechanisms and  antibacterial properties of silver nanoparticles are well known, but the effects of gold nanoparticles, especially gold Nano bipyramids, are not considered. In this research, we synthesized gold nanobipyramids (NBPs) by seed mediated method using surfactant cetyltrimethylammonium bromide (CTAB). After preparing, gold nanobipyramids is removed CTAB and modified the surface using polyethylene glycol, polyvinyl alcohol and chitosan as the stabilizers. Besides, antibacterial effects of gold nanobipyramids on both Escherichia coli (Gram negative) and Staphylococcus aureus (Gram positive) are investigated in this paper. The results show that gold nanobipyramids have good antibacterial activities even at low concentration. The optimal concentration of stabilizers and gold nanobipyramids in antibacterial activities are also studied in this paper

    Synthesis and Characterization of Silver Nanoplates by a Seed-mediated Method

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    Silver nanoplates (SNPs) having different size were synthesized by a seed-mediated method. The seeds -silver nanoparticles with 4 – 6 nm diameters were synthesized first by reducing silver nitrate with sodium borohydride in the present of Trisodium Citrate and Hydrogen peroxide. Then these seeds were developed by continue reducing Ag+^+ ions with various amount of L-Ascorbic acid to form SNPs. Our analysis showed that the concentratrion of L-Ascorbic acid, a secondary reducing agent, played an important role to form SNPs. In addition, the size and in-plane dipole plasmon resonance wavelenght of silver nanoplates were increased when the concentration of added silver nitrate increased. The characterization of SNPs were studied by UV-Vis, FE-SEM, EDS and TEM methods

    Socializing One Health: an innovative strategy to investigate social and behavioral risks of emerging viral threats

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    In an effort to strengthen global capacity to prevent, detect, and control infectious diseases in animals and people, the United States Agency for International Development’s (USAID) Emerging Pandemic Threats (EPT) PREDICT project funded development of regional, national, and local One Health capacities for early disease detection, rapid response, disease control, and risk reduction. From the outset, the EPT approach was inclusive of social science research methods designed to understand the contexts and behaviors of communities living and working at human-animal-environment interfaces considered high-risk for virus emergence. Using qualitative and quantitative approaches, PREDICT behavioral research aimed to identify and assess a range of socio-cultural behaviors that could be influential in zoonotic disease emergence, amplification, and transmission. This broad approach to behavioral risk characterization enabled us to identify and characterize human activities that could be linked to the transmission dynamics of new and emerging viruses. This paper provides a discussion of implementation of a social science approach within a zoonotic surveillance framework. We conducted in-depth ethnographic interviews and focus groups to better understand the individual- and community-level knowledge, attitudes, and practices that potentially put participants at risk for zoonotic disease transmission from the animals they live and work with, across 6 interface domains. When we asked highly-exposed individuals (ie. bushmeat hunters, wildlife or guano farmers) about the risk they perceived in their occupational activities, most did not perceive it to be risky, whether because it was normalized by years (or generations) of doing such an activity, or due to lack of information about potential risks. Integrating the social sciences allows investigations of the specific human activities that are hypothesized to drive disease emergence, amplification, and transmission, in order to better substantiate behavioral disease drivers, along with the social dimensions of infection and transmission dynamics. Understanding these dynamics is critical to achieving health security--the protection from threats to health-- which requires investments in both collective and individual health security. Involving behavioral sciences into zoonotic disease surveillance allowed us to push toward fuller community integration and engagement and toward dialogue and implementation of recommendations for disease prevention and improved health security

    INVESTIGATION OF COUPLED EFFECTS OF TEMPERATURE AND RELATIVE HUMIDITY ON DYNAMIC PERFORMANCE OF MEMS CANTILEVER RESONATORS IN GAS RAREFACTION

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    The modified molecular gas lubrication (MMGL) equation with the effective viscosity of moist air is utilized to solve for the squeeze film damping (SFD) problem on the dynamic performance of MEMS cantilever resonators. Thus, the coupled effects of temperature and relative humidity are discussed on the Q-factors of MEMS cantilever resonators in a wide range of gas rarefaction (pressure, p and accommodation coefficients, ACs) and resonant mode of vibration. The results showed that the Q-factor of moist air decreases more significantly as temperature and relative humidity increase at higher gas rarefaction (lower p, and ACs) conditions.

    Photochemical Synthesis of Silver Nanodecahedrons under Blue LED Irradiation and Their SERS Activity

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    Silver nanodecahedrons were successfully synthesized by a photochemical method under irradiation of blue light-emitting diodes (LEDs). The formation of silver nanodecahedrons at different LED irradiation times (0–72 h) was thoroughly investigated by employing different characterization methods such as ultraviolet–visible spectroscopy (UV–Vis), transmission electron microscopy (TEM), and Raman spectroscopy. The results showed that silver nanodecahedrons (AgNDs) were formed from silver nanoseeds after 6 h of LED irradiation. The surface-enhanced Raman scattering (SERS) effects of the synthesized AgNDs were also studied in comparison with those of spherical silver nanoparticles in the detection of 4-mercapto benzoic acid. Silver nanodecahedrons with a size of 48 nm formed after 48 h of LED irradiation displayed stronger SERS properties than spherical nanoparticles because of electromagnetic enhancement. The formation mechanism of silver nanodecahedrons is also reported in our study. The results showed that multihedral silver nanoseeds favored the formation of silver nanodecahedrons

    One-Pot, Surfactant-Free Synthesis of Gold Nanostars and Evaluation of Their Antibacterial Effects against Propionibacterium acnes

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    Anisotropic gold nanoparticles, especially gold nanostars, are used in many fields of biomedical applications such as sensing, targeted drug delivery, and diagnostic and photothermal therapy. In this study, we introduced a novel application of gold nanostars as an antimicrobial agent. While spherical gold nanoparticles have an inappreciable effect, gold nanostars exhibit significant antibacterial activity. Besides, the seed-mediated method, a conventional technique for preparing gold nanostars, is rather complex and toxic to human and environment due to unsafe synthesized materials such as surfactants and reducers. In recent years, green chemistry for nanoparticle synthesis is attractive because of its advantages. Instead of the seed-mediated procedure, we present a facile and green procedure to synthesize gold nanostars using ascorbic acid as a reductant and chitosan as a directing-growth agent. The influences of reacting parameters were evaluated to determine the optimal conditions. Star-shaped gold nanoparticles were successfully synthesized with average size tunning from 137.0±20.7 nm to 281.9±25.8 nm of the core and 14.0±4.4 nm to 54.2±11.9 nm of branches. Antibacterial activity against Propionibacterium acnes of gold nanostars was also investigated. Propionibacterium acnes is one of the main reasons causing acne vulgaris. The antibacterial test was evaluated by the plate count and well diffusion method. The results showed a significant effect that gold nanostars could be the prospective agent for replacing antibiotics in acne treatment
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