Some aspects of nanocrystalline nickel and zinc ferrites processed using microemulsion technique

Nanocrystalline nickel and zinc ferrites synthesised using a microemulsion technique were characterised by high resolution transmission electron microscopy and vibrating sample magnetometry. A narrow and uniform distribution of crystals of size range 5 – 8 nm, distinguished by a clear lack of saturation magnetisation at 9 kOe, were obtained. Also, no coercivity or remanence was observed.

Strengthening mechanisms in thermomechanically processed NbTi-microalloyed steel

The effect of deformation temperature on microstructure and mechanical properties was investigated for thermomechanically processed NbTi-microalloyed steel with ferrite-pearlite microstructure. With a decrease in the finish deformation temperature at 1348 K to 1098 K (1075 °C to 825 °C) temperature range, the ambient temperature yield stress did not vary significantly, work hardening rate decreased, ultimate tensile strength decreased, and elongation to failure increased. These variations in mechanical properties were correlated to the variations in microstructural parameters (such as ferrite grain size, solid solution concentrations, precipitate number density and dislocation density). Calculations based on the measured microstructural parameters suggested the grain refinement, solid solution strengthening, precipitation strengthening, and work hardening contributed up to 32 pct, up to 48 pct, up to 25 pct, and less than 3 pct to the yield stress, respectively. With a decrease in the finish deformation temperature, both the grain size strengthening and solid solution strengthening increased, the precipitation strengthening decreased, and the work hardening contribution did not vary significantly

EBSD characterization of cryogenically rolled type 321 austenitic stainless steel

Electron backscatter diffraction was applied to investigate microstructure evolution during cryogenic rolling of type 321 metastable austenitic stainless steel. As expected, rolling promoted deformation-induced martensitic transformation which developed preferentially in deformation bands. Because a large fraction of the imposed strain was accommodated by deformation banding, grain refinement in the parent austenite phase was minimal. The martensitic transformation was found to follow a general orientation relationship, {111}γ||{0001}ε||{110}α′ and 〈110〉γ||〈11-20〉ε||〈111〉α′, and was characterized by noticeable variant selection

Martensite-to-austenite reversion and recrystallization in cryogenically-rolled type 321 metastable austenitic steel

The annealing behavior of cryogenically-rolled type 321 metastable austenitic steel was established. Cryogenic deformation gave rise to martensitic transformation which developed preferentially within deformation bands. Subsequent annealing in the range of 600 C to 700 C resulted in reversion of the strain-induced martensite to austenite. At 800 C, the reversion was followed by static recrystallization. At relatively-low temperatures, the reversion was characterized by a very strong variant selection, which led to the restoration of the crystallographic orientation of the coarse parent austenite grains. An increase in the annealing temperature relaxed the variant-selection tendency and provided subsequent recrystallization thus leading to significant grain refinement. Nevertheless, a significant portion of the original coarse grains was found to be untransformed and therefore the fine-grain structure was fairly heterogeneous

Investigation of the behaviour of scratched metal electrodes

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Comparative study on effects of annealing temperature on microstructures and mechanical properties of high-Al low-Si steel

We elucidate here profound effects of quenching and partitioning process after partial (IQP) or full austenitization (FQP) on the microstructure and mechanical properties of high strength hot-dip galvanized steel with high Al and low Si content. The results showed that the FQP steel contains 3.38% vol.% retained austenite with mainly film-like morphology, while the IQP steel mainly consists of 6.44–8.13 vol.% retained austenite with block shape. Additionally, retained austenite in the IQP sample transforms into martensite more easily duo to higher nucleation rate, which means lower austenite stability. A combination of various austenite grain size and morphology make the TRIP effect throughout the whole deformation process and increased the elongation for IQP sample. When the steel was treated by annealing temperature of 967 °C, partitioning temperature and time of 460 °C and 100 s respectively, the steel exhibited excellent mechanical properties with tensile strength of 754 MPa, total elongation of 27% and the product of strength and ductility exceeds 20 GPa%. The proposed content in the present study demonstrates compatibility with the continuous hot-dip galvanizing process